N-(2-Methyl-1-phenyl-propenyl)-formimidic acid sec-butyl ester

Base Information

• Chemical Name: N-(2-Methyl-1-phenyl-propenyl)-formimidic acid sec-butyl ester
• CAS No.: 133682-33-4
• Molecular Formula: C₁₅H₂₁NO
• Molecular Weight: 231.338
• Mol file: 133682-33-4.mol

Synonyms:N-(2-Methyl-1-phenyl-propenyl)-formimidic acid sec-butyl ester

Chemical Property of N-(2-Methyl-1-phenyl-propenyl)-formimidic acid sec-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N-(2-Methyl-1-phenyl-propenyl)-formimidic acid sec-butyl ester

There total 1 articles about N-(2-Methyl-1-phenyl-propenyl)-formimidic acid sec-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

tri-sec-butyl orthoformate (16754-48-6,17159-00-1) + 2-methyl-1-phenylpropan-1-imine (35129-66-9) → N-(2-Methyl-1-phenyl-propenyl)-formimidic acid sec-butyl ester (133682-33-4)

Guidance literature:

toluene-4-sulfonic acid; at 150 - 160 ℃; for 0.25h;

DOI:10.1246/bcsj.64.766

Reference yield: 15.0%

N-(2-Methyl-1-phenyl-propenyl)-formimidic acid sec-butyl ester (133682-33-4) + chloroacetyl chloride (79-04-9) → N-sec-Butoxymethyl-2-chloro-N-(2-methyl-1-phenyl-propenyl)-acetamide (141070-82-8)

Guidance literature:

With trichlorosilane; In benzene; at 20 - 50 ℃;

DOI:10.1246/bcsj.65.674

upstream raw materials:

tri-sec-butyl orthoformate

2-methyl-1-phenylpropan-1-imine

Downstream raw materials:

N-sec-Butoxymethyl-2-chloro-N-(2-methyl-1-phenyl-propenyl)-acetamide