C₁₇H₁₈⁽²⁾H₃NO₇

Base Information

Chemical Name:C₁₇H₁₈⁽²⁾H₃NO₇
CAS No.:1597585-60-8
Molecular Formula:C₁₇H₂₁NO₇
Molecular Weight:354.332
Hs Code.:

C<sub>17</sub>H<sub>18</sub><sup>(2)</sup>H<sub>3</sub>NO<sub>7</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₈⁽²⁾H₃NO₇

Chemical Property:

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Technology Process of C₁₇H₁₈⁽²⁾H₃NO₇

There total 4 articles about C₁₇H₁₈⁽²⁾H₃NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (3R)-1-ethyl 6-isopropyl 2-nitro-5-oxo-3-phenylhexanedioate

: 1597585-60-8
C₁₇H₁₈⁽²⁾H₃NO₇

Guidance literature:: With BF₄*C₈H₁₂CuN₄⁽¹⁺⁾; (S)-2-((2-(hydroxydi-p-tolylmethyl)pyrrolidin-1-yl)methyl)-6-(trifluoromethyl)phenol; water-d2; potassium carbonate; In toluene; at 20 ℃; Reagent/catalyst; Inert atmosphere;
DOI:10.1002/chem.201303512

Reference yield:

: 111160-44-2
i-propyl 2-oxo-4-phenylbut-3-enoate

: 1597585-60-8
C₁₇H₁₈⁽²⁾H₃NO₇

Guidance literature:: Multi-step reaction with 2 steps

1.1: BF₄*C₈H₁₂CuN₄⁽¹⁺⁾; lithium carbonate; (S)-2-((2-(hydroxydi-p-tolylmethyl)pyrrolidin-1-yl)methyl)-6-(trifluoromethyl)phenol / toluene / 1 h / 0 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: water-d2; BF₄*C₈H₁₂CuN₄⁽¹⁺⁾; (S)-2-((2-(hydroxydi-p-tolylmethyl)pyrrolidin-1-yl)methyl)-6-(trifluoromethyl)phenol; potassium carbonate / toluene / 20 °C / Inert atmosphere

With BF₄*C₈H₁₂CuN₄⁽¹⁺⁾; (S)-2-((2-(hydroxydi-p-tolylmethyl)pyrrolidin-1-yl)methyl)-6-(trifluoromethyl)phenol; water-d2; lithium carbonate; potassium carbonate; In toluene; 1.1: |Michael Addition / 1.2: |Michael Addition;
DOI:10.1002/chem.201303512

Reference yield:

: 100-52-7
benzaldehyde

: 1597585-60-8
C₁₇H₁₈⁽²⁾H₃NO₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / methanol / 1 h / 30 °C

2.1: acetyl chloride / 0 - 20 °C / Reflux

3.1: BF₄*C₈H₁₂CuN₄⁽¹⁺⁾; lithium carbonate; (S)-2-((2-(hydroxydi-p-tolylmethyl)pyrrolidin-1-yl)methyl)-6-(trifluoromethyl)phenol / toluene / 1 h / 0 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

4.1: water-d2; BF₄*C₈H₁₂CuN₄⁽¹⁺⁾; (S)-2-((2-(hydroxydi-p-tolylmethyl)pyrrolidin-1-yl)methyl)-6-(trifluoromethyl)phenol; potassium carbonate / toluene / 20 °C / Inert atmosphere

With BF₄*C₈H₁₂CuN₄⁽¹⁺⁾; (S)-2-((2-(hydroxydi-p-tolylmethyl)pyrrolidin-1-yl)methyl)-6-(trifluoromethyl)phenol; water-d2; lithium carbonate; potassium carbonate; acetyl chloride; potassium hydroxide; In methanol; toluene; 3.1: |Michael Addition / 3.2: |Michael Addition;
DOI:10.1002/chem.201303512