1-cyclopropyl-1-methyl-ethylamine hydrochloride

Base Information

• Chemical Name: 1-cyclopropyl-1-methyl-ethylamine hydrochloride
• CAS No.: 17397-13-6
• Molecular Formula: C₆H₁₃N*ClH
• Molecular Weight: 135.637
• Hs Code.: 2921309990
• Mol file: 17397-13-6.mol

Synonyms:

Chemical Property of 1-cyclopropyl-1-methyl-ethylamine hydrochloride

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

2-Cyclopropylpropan-2-amineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-cyclopropyl-1-methyl-ethylamine hydrochloride

There total 3 articles about 1-cyclopropyl-1-methyl-ethylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

methyllithium (917-54-4) + cyclopropropanecarbonitrile (5500-21-0) → 1-cyclopropyl-1-methyl-ethylamine hydrochloride (17397-13-6)

Guidance literature:

methyllithium; With cerium(III) chloride; In tetrahydrofuran; at -80 ℃; for 2h;

cyclopropropanecarbonitrile; In tetrahydrofuran; at -80 - 20 ℃; for 26h;

With hydrogenchloride; In water; ethyl acetate; Temperature;

Reference yield:

N-chlorosulfonyl-1-cyclopropyl-1-methylethylamine → 1-cyclopropyl-1-methyl-ethylamine hydrochloride (17397-13-6)

Guidance literature:

N-chlorosulfonyl-1-cyclopropyl-1-methylethylamine; With water; sodium hydroxide; In dichloromethane; for 2.5h;

With hydrogenchloride; In ethyl acetate;

Reference yield:

Cyclopropyl methyl ketone (765-43-5) → 1-cyclopropyl-1-methyl-ethylamine hydrochloride (17397-13-6)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran / 3.5 h / -50 - 20 °C / Inert atmosphere

2: dichloromethane / 3 h / 5 °C

3: sodium hydroxide; water / dichloromethane / 2.5 h

With water; sodium hydroxide; In tetrahydrofuran; dichloromethane;

upstream raw materials:

Cyclopropyl methyl ketone

methyllithium

cyclopropropanecarbonitrile

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