Technology Process of C26H28F2N4O4S
There total 11 articles about C26H28F2N4O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium chloride;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride / ethyl acetate / 1 h / 0 - 20 °C
2: oxalyl dichloride; N,N-dimethyl-formamide / N,N-dimethyl-formamide; toluene / 2 h / 0 - 20 °C / Inert atmosphere
3: chloroform / 16 h / 20 °C
4: 1-methyl-1H-imidazole / 65 °C
5: lithium chloride / N,N-dimethyl-formamide / 3 h / 100 °C
With
1-methyl-1H-imidazole; hydrogenchloride; oxalyl dichloride; N,N-dimethyl-formamide; lithium chloride;
In
chloroform; ethyl acetate; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -70 °C / Inert atmosphere
1.2: 1 h / -70 °C
2.1: hydrogenchloride / ethyl acetate / 1 h / 0 - 20 °C
3.1: oxalyl dichloride; N,N-dimethyl-formamide / N,N-dimethyl-formamide; toluene / 2 h / 0 - 20 °C / Inert atmosphere
4.1: chloroform / 16 h / 20 °C
5.1: 1-methyl-1H-imidazole / 65 °C
6.1: lithium chloride / N,N-dimethyl-formamide / 3 h / 100 °C
With
1-methyl-1H-imidazole; hydrogenchloride; oxalyl dichloride; N,N-dimethyl-formamide; lithium chloride; lithium hexamethyldisilazane;
In
tetrahydrofuran; chloroform; ethyl acetate; N,N-dimethyl-formamide; toluene;