Technology Process of C47H48Cl3NO13
There total 11 articles about C47H48Cl3NO13 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 3(CH2)3>4N(HSO4), NaOH / CH2Cl2
2: 73.7 percent / N-iodosuccinimide, triflic acid / CH2Cl2
3: 62 percent / trichloroacetic acid / CH2Cl2
4: DBU / CH2Cl2
With
sodium hydroxide; N-iodo-succinimide; trifluorormethanesulfonic acid; tetrabutylammonium perchlorate; 1,8-diazabicyclo[5.4.0]undec-7-ene; trichloroacetic acid;
In
dichloromethane;
DOI:10.1016/S0957-4166(98)00494-7
- Guidance literature:
-
Multi-step reaction with 6 steps
1: NaH / dimethylformamide
2: aq. AcOH
3: pyridine
4: 73.7 percent / N-iodosuccinimide, triflic acid / CH2Cl2
5: 62 percent / trichloroacetic acid / CH2Cl2
6: DBU / CH2Cl2
With
pyridine; N-iodo-succinimide; trifluorormethanesulfonic acid; sodium hydride; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; trichloroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0957-4166(98)00494-7
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 45 percent / p-TsOH / dimethylformamide / 80 °C
2: NaH / dimethylformamide
3: HCl, MeOH / CH2Cl2
4: 3(CH2)3>4N(HSO4), NaOH / CH2Cl2
5: 73.7 percent / N-iodosuccinimide, triflic acid / CH2Cl2
6: 62 percent / trichloroacetic acid / CH2Cl2
7: DBU / CH2Cl2
With
hydrogenchloride; methanol; sodium hydroxide; N-iodo-succinimide; trifluorormethanesulfonic acid; tetrabutylammonium perchlorate; sodium hydride; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; trichloroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0957-4166(98)00494-7