Bis(triphenylmethyl)tetrasulfane

Base Information

• Chemical Name: Bis(triphenylmethyl)tetrasulfane
• CAS No.: 23264-36-0
• Molecular Formula: C₃₈H₃₀S₄
• Molecular Weight: 614.92
• Mol file: 23264-36-0.mol

Synonyms:

Chemical Property of Bis(triphenylmethyl)tetrasulfane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Bis(triphenylmethyl)tetrasulfane

There total 7 articles about Bis(triphenylmethyl)tetrasulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

n-butanethiol (109-79-5) + Chloro(triphenylmethyl)tetrasulfane (152216-82-5) → Bis(triphenylmethyl)tetrasulfane (23264-36-0) + n-Butyl(triphenylmethyl)tetrasulfane

Guidance literature:

In diethyl ether; for 8h;

DOI:10.1021/jo00083a022

Reference yield:

α,α-diphenylbenzenemethanesulfenyl chloride (35572-83-9) → Bis(triphenylmethyl)tetrasulfane (23264-36-0) + Butyl(triphenylmethyl)disulfane

Guidance literature:

With butyl magnesium bromide; In diethyl ether; at 0 ℃; for 1h; Yields of byproduct given;

DOI:10.1021/jo00083a022

Reference yield:

triphenylmethanedithiosulfenyl chloride (152216-81-4) → Bis(triphenylmethyl)trisulfane (58451-52-8) + Bis(triphenylmethyl)tetrasulfane (23264-36-0) + Butyl(triphenylmethyl)trisulfane

Guidance literature:

With butyl magnesium bromide; In diethyl ether; at 0 ℃; for 1h; Yields of byproduct given;

DOI:10.1021/jo00083a022

upstream raw materials:

n-butanethiol

Chloro(triphenylmethyl)tetrasulfane

α,α-diphenylbenzenemethanesulfenyl chloride

triphenylmethanedithiosulfenyl chloride

Refernces