2--dithiocarbazinsaeure-methylester

Base Information

• Chemical Name: 2--dithiocarbazinsaeure-methylester
• CAS No.: 15095-41-7
• Molecular Formula: C₁₀H₁₂N₂OS₂
• Molecular Weight: 240.35
• Mol file: 15095-41-7.mol

Synonyms:

Chemical Property of 2--dithiocarbazinsaeure-methylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2--dithiocarbazinsaeure-methylester

There total 1 articles about 2--dithiocarbazinsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + 2-phenylacetylhydrazine (937-39-3) + methyl iodide (74-88-4) → 2--dithiocarbazinsaeure-methylester (15095-41-7)

Guidance literature:

With triethylamine; In ethanol; at 20 ℃;

DOI:10.1080/10426500008045234

Reference yield:

2--dithiocarbazinsaeure-methylester (15095-41-7) → 2-(3-Benzyl-5-methylsulfanyl-[1,2,4]triazol-4-yl)-ethanol (96134-39-3)

Guidance literature:

Multi-step reaction with 2 steps

1: Heating

2: 64 percent / KOH / methanol / Heating

With potassium hydroxide; In methanol;

DOI:10.1080/10426500008045234

Reference yield:

2--dithiocarbazinsaeure-methylester (15095-41-7) → 2-(3-benzyl-[1,2,4]triazol-4-yl)-ethanol

Guidance literature:

Multi-step reaction with 2 steps

1: Heating

2: 40 percent / Ra-Ni / ethanol / 4 h / Heating

With Ra-Ni; In ethanol;

DOI:10.1080/10426500008045234

upstream raw materials:

carbon disulfide

2-phenylacetylhydrazine

methyl iodide

Downstream raw materials:

2-(3-Benzyl-5-methylsulfanyl-[1,2,4]triazol-4-yl)-ethanol