2-amino-9-(2,3,5-triphenylmethoxy-β-D-arabinofuranosyl)purine

Base Information

Chemical Name:2-amino-9-(2,3,5-triphenylmethoxy-β-D-arabinofuranosyl)purine
CAS No.:847654-59-5
Molecular Formula:C₃₁H₃₁N₅O₄
Molecular Weight:537.618
Hs Code.:

Synonyms:

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Chemical Property of 2-amino-9-(2,3,5-triphenylmethoxy-β-D-arabinofuranosyl)purine

Chemical Property:

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Technology Process of 2-amino-9-(2,3,5-triphenylmethoxy-β-D-arabinofuranosyl)purine

There total 2 articles about 2-amino-9-(2,3,5-triphenylmethoxy-β-D-arabinofuranosyl)purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52554-29-7
2,3,5-tri-O-benzyl-α- and β-D-arabinofuranosyl chlorides

: 847654-59-5
2-amino-9-(2,3,5-triphenylmethoxy-β-D-arabinofuranosyl)purine

Guidance literature:: Multi-step reaction with 2 steps

1: 78.5 percent / moleucular sieves 4A / 1,2-dichloro-ethane / 144 h / 20 °C

2: H₂; aq. NH₃ / Pd/C / methanol; tetrahydrofuran / 4 h / 20 °C / 2585.74 Torr

With ammonium hydroxide; 4 A molecular sieve; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2004.11.029

Reference yield:

: 160549-10-0
2,3,5-tri-O-benzyl-D-arabinofuranose

: 847654-59-5
2-amino-9-(2,3,5-triphenylmethoxy-β-D-arabinofuranosyl)purine

Guidance literature:: Multi-step reaction with 4 steps

1: 98.5 percent / pyridine / 4 h / 20 °C

2: 87.1 percent / HCl(gas) / CH₂Cl₂ / 3 h / 0 °C

3: 78.5 percent / moleucular sieves 4A / 1,2-dichloro-ethane / 144 h / 20 °C

4: H₂; aq. NH₃ / Pd/C / methanol; tetrahydrofuran / 4 h / 20 °C / 2585.74 Torr

With pyridine; hydrogenchloride; ammonium hydroxide; 4 A molecular sieve; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2004.11.029