Diisopropyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(2-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-6-oxo-1,6-dihydro-purin-9-yl)-2-methoxy-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester hexadecyl ester

Base Information

Chemical Name:Diisopropyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(2-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-6-oxo-1,6-dihydro-purin-9-yl)-2-methoxy-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester hexadecyl ester
CAS No.:132470-72-5
Molecular Formula:C₅₅H₇₉N₆O₉P
Molecular Weight:999.241
Hs Code.:

Diisopropyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(2-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-6-oxo-1,6-dihydro-purin-9-yl)-2-methoxy-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester hexadecyl ester

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Chemical Property of Diisopropyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(2-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-6-oxo-1,6-dihydro-purin-9-yl)-2-methoxy-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester hexadecyl ester

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Technology Process of Diisopropyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(2-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-6-oxo-1,6-dihydro-purin-9-yl)-2-methoxy-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester hexadecyl ester

There total 4 articles about Diisopropyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(2-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-6-oxo-1,6-dihydro-purin-9-yl)-2-methoxy-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester hexadecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 132470-71-4
hexadecyloxybis(diisopropylamino)phosphine

: 98151-72-5
2-N-(4,4'-dimethoxytrityl)-2',3'-di-O-methoxymethyleneguanosine

: 132470-72-5
Diisopropyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(2-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-6-oxo-1,6-dihydro-purin-9-yl)-2-methoxy-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester hexadecyl ester

Guidance literature:: With 1H-tetrazole; In 1,4-dioxane; diethyl ether; for 2h; Ambient temperature;

Reference yield:

: 36653-82-4,124-29-8
1-Hexadecanol

: 132470-72-5
Diisopropyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(2-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-6-oxo-1,6-dihydro-purin-9-yl)-2-methoxy-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester hexadecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / diethyl ether / 1 h / -30 deg C -> r.t.

2: 47 percent / 1-H-tetrazole / dioxane; diethyl ether / 2 h / Ambient temperature

With 1H-tetrazole; triethylamine; In 1,4-dioxane; diethyl ether;

Reference yield:

: 56183-63-2
bis(diisopropylamino)chlorophosphine

: 132470-72-5
Diisopropyl-phosphoramidous acid (3aR,4R,6R,6aR)-6-(2-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-6-oxo-1,6-dihydro-purin-9-yl)-2-methoxy-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester hexadecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / diethyl ether / 1 h / -30 deg C -> r.t.

2: 47 percent / 1-H-tetrazole / dioxane; diethyl ether / 2 h / Ambient temperature

With 1H-tetrazole; triethylamine; In 1,4-dioxane; diethyl ether;