(+/-)-1,5,6-tri-O-benzyl-myo-inositol

Base Information

Chemical Name:(+/-)-1,5,6-tri-O-benzyl-myo-inositol
CAS No.:131146-93-5
Molecular Formula:C₂₇H₃₀O₆
Molecular Weight:450.532
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-1,5,6-tri-O-benzyl-myo-inositol

Chemical Property:

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Technology Process of (+/-)-1,5,6-tri-O-benzyl-myo-inositol

There total 17 articles about (+/-)-1,5,6-tri-O-benzyl-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 131146-92-4
(+/-)-1,5,6-tri-O-benzyl-4-O-(prop-1-enyl)-myo-inositol

: 131146-93-5,131233-69-7,131233-70-0,145772-95-8
(+/-)-1,5,6-tri-O-benzyl-myo-inositol

Guidance literature:: With hydrogenchloride; In methanol; for 0.5h; Heating;
DOI:10.1016/0008-6215(90)80132-M

Reference yield:

: 100-39-0
benzyl bromide

: 131146-93-5,131233-69-7,131233-70-0,145772-95-8
(+/-)-1,5,6-tri-O-benzyl-myo-inositol

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / dimethylformamide

2: M HCl / methanol / 0.5 h / Heating

3: 1) tetrabutylammonium bromide, dibutyltin oxide / 1) toluene, 2 h, reflux, 2) 2 h, reflux

4: toluene-p-sulphonic acid monohydrate / 10percent Pd-C / ethanol; H₂O / 11 h / Heating

With hydrogenchloride; tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)80132-M

Reference yield:

: 58706-24-4,58769-25-8,98974-91-5,111466-16-1
(±)-3-O-benzyl-1,2:4,5-di-O-isopropylidene-myo-inositol

: 131146-93-5,131233-69-7,131233-70-0,145772-95-8
(+/-)-1,5,6-tri-O-benzyl-myo-inositol

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydride / dimethylformamide

2: 49 percent / toluene-p-sulphonic acid monohydrate / acetone; H₂O / 0.75 h / 25 °C

3: sodium hydride / dimethylformamide

4: M HCl / methanol / 0.75 h / Heating

5: potassium tert-butoxide / dimethylsulfoxide / 2 h / 50 °C

6: 78 percent / M HCl / methanol / 0.5 h / Heating

With hydrogenchloride; potassium tert-butylate; sodium hydride; toluene-4-sulfonic acid; In methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0008-6215(90)80132-M