C₂₅H₂₄N₄O₃S

Base Information

Chemical Name:C₂₅H₂₄N₄O₃S
CAS No.:1426154-05-3
Molecular Formula:C₂₅H₂₄N₄O₃S
Molecular Weight:460.557
Hs Code.:

C<sub>25</sub>H<sub>24</sub>N<sub>4</sub>O<sub>3</sub>S

Synonyms:

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Chemical Property of C₂₅H₂₄N₄O₃S

Chemical Property:

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Technology Process of C₂₅H₂₄N₄O₃S

There total 7 articles about C₂₅H₂₄N₄O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1101819-82-2
4-{2-chloro-6-[1-(phenylsulfonyl)cyclopropyl]pyrimidin-4-yl}morpholine

: 220465-43-0
indole-4-boronic acid

: 1426154-05-3
C₂₅H₂₄N₄O₃S

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate; In 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide; at 95 ℃; for 1h; Microwave irradiation;
DOI:10.1021/jm301859s

Reference yield:

: 107973-01-3
Methyl Ester of 6-Morpholino-2-chloropyrimidine-4-carboxylic acid

: 1426154-05-3
C₂₅H₂₄N₄O₃S

Guidance literature:: Multi-step reaction with 6 steps

1: lithium borohydride / tetrahydrofuran / 3.5 h / -5 - 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

3: sodium iodide / acetone / 2 h / 20 °C / Inert atmosphere

4: acetonitrile / 3 h / 80 °C / Inert atmosphere

5: sodium hydroxide; tetrabutylammomium bromide / water; dichloromethane; toluene / 18 h / 60 °C / Inert atmosphere

6: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; ethanol / 1 h / 95 °C / Microwave irradiation

With bis-triphenylphosphine-palladium(II) chloride; lithium borohydride; tetrabutylammomium bromide; sodium carbonate; N-ethyl-N,N-diisopropylamine; sodium iodide; sodium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; 6: |Suzuki Coupling;
DOI:10.1021/jm301859s

Reference yield:

: 1101818-27-2
(2-chloro-6-morpholin-4-ylpyrimidin-4-yl)methyl methanesulfonate

: 1426154-05-3
C₂₅H₂₄N₄O₃S

Guidance literature:: Multi-step reaction with 4 steps

1: sodium iodide / acetone / 2 h / 20 °C / Inert atmosphere

2: acetonitrile / 3 h / 80 °C / Inert atmosphere

3: sodium hydroxide; tetrabutylammomium bromide / water; dichloromethane; toluene / 18 h / 60 °C / Inert atmosphere

4: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; ethanol / 1 h / 95 °C / Microwave irradiation

With bis-triphenylphosphine-palladium(II) chloride; tetrabutylammomium bromide; sodium carbonate; sodium iodide; sodium hydroxide; In 1,2-dimethoxyethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; 4: |Suzuki Coupling;
DOI:10.1021/jm301859s