2,3,4-tri-O-benzoyl-5-thio-α-L-fucopyranosyl dibenzyl phosphate

Base Information

Chemical Name:2,3,4-tri-O-benzoyl-5-thio-α-L-fucopyranosyl dibenzyl phosphate
CAS No.:182694-23-1
Molecular Formula:C₄₁H₃₇O₁₀PS
Molecular Weight:752.779
Hs Code.:

Synonyms:

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Chemical Property of 2,3,4-tri-O-benzoyl-5-thio-α-L-fucopyranosyl dibenzyl phosphate

Chemical Property:

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Technology Process of 2,3,4-tri-O-benzoyl-5-thio-α-L-fucopyranosyl dibenzyl phosphate

There total 5 articles about 2,3,4-tri-O-benzoyl-5-thio-α-L-fucopyranosyl dibenzyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-88-4
benzoyl chloride

: 182694-23-1
2,3,4-tri-O-benzoyl-5-thio-α-L-fucopyranosyl dibenzyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 20 °C

2: HBr; AcOH / CH₂Cl₂ / 2 h / 20 °C

3: 112 mg / benzene / 1 h / Heating

With pyridine; hydrogen bromide; acetic acid; In dichloromethane; benzene;
DOI:10.1021/jo0300035

Reference yield:

: 1,2,3,4-tetra-O-acetyl-5-thio-L-fucopyranose

: 182694-23-1
2,3,4-tri-O-benzoyl-5-thio-α-L-fucopyranosyl dibenzyl phosphate

Guidance literature:: Multi-step reaction with 4 steps

1: NaOMe / methanol

2: pyridine / 20 °C

3: HBr; AcOH / CH₂Cl₂ / 2 h / 20 °C

4: 112 mg / benzene / 1 h / Heating

With pyridine; hydrogen bromide; sodium methylate; acetic acid; In methanol; dichloromethane; benzene;
DOI:10.1021/jo0300035

Reference yield:

: 5-Thio-L-fucopyranose

: 182694-23-1
2,3,4-tri-O-benzoyl-5-thio-α-L-fucopyranosyl dibenzyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 20 °C

2: HBr; AcOH / CH₂Cl₂ / 2 h / 20 °C

3: 112 mg / benzene / 1 h / Heating

With pyridine; hydrogen bromide; acetic acid; In dichloromethane; benzene;
DOI:10.1021/jo0300035