Technology Process of C13H7ClF5NO5S
There total 7 articles about C13H7ClF5NO5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 99 percent / H2 / Raney nickel / ethanol
2.1: NCS / acetonitrile
3.1: t-BuONO; CuCl2 / acetonitrile
4.1: KOH
4.2: K2CO3; CsF / dimethylsulfoxide
5.1: SOCl2
6.1: KNO3; conc. H2SO4 / 1,2-dichloro-ethane
7.1: aq. NaOH
With
potassium hydroxide; sodium hydroxide; N-chloro-succinimide; thionyl chloride; tert.-butylnitrite; sulfuric acid; hydrogen; potassium nitrate; copper dichloride;
nickel;
In
ethanol; 1,2-dichloro-ethane; acetonitrile;
DOI:10.2533/000942904777678172
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: NCS / acetonitrile
2.1: t-BuONO; CuCl2 / acetonitrile
3.1: KOH
3.2: K2CO3; CsF / dimethylsulfoxide
4.1: SOCl2
5.1: KNO3; conc. H2SO4 / 1,2-dichloro-ethane
6.1: aq. NaOH
With
potassium hydroxide; sodium hydroxide; N-chloro-succinimide; thionyl chloride; tert.-butylnitrite; sulfuric acid; potassium nitrate; copper dichloride;
In
1,2-dichloro-ethane; acetonitrile;
DOI:10.2533/000942904777678172
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: KOH
1.2: K2CO3; CsF / dimethylsulfoxide
2.1: SOCl2
3.1: KNO3; conc. H2SO4 / 1,2-dichloro-ethane
4.1: aq. NaOH
With
potassium hydroxide; sodium hydroxide; thionyl chloride; sulfuric acid; potassium nitrate;
In
1,2-dichloro-ethane;
DOI:10.2533/000942904777678172
