Technology Process of C16H15NO4S
There total 4 articles about C16H15NO4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-(4-methylphenyl)-1-(4-methanesulfonylphenyl)ethanone;
With
sodium methylate;
In
methanol;
at 20 ℃;
With
n-Butyl nitrite;
In
methanol;
at 20 ℃;
DOI:10.1016/j.bmc.2013.12.002
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic anhydride / phosphoric acid / 0.08 h / 20 °C
2.1: Oxone / methanol; tetrahydrofuran / 4 h / 20 °C
3.1: sodium methylate / methanol / 20 °C
3.2: 20 °C
With
sodium methylate; trifluoroacetic anhydride;
In
tetrahydrofuran; methanol; phosphoric acid;
DOI:10.1016/j.bmc.2013.12.002
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic anhydride / phosphoric acid / 0.08 h / 20 °C
2.1: Oxone / methanol; tetrahydrofuran / 4 h / 20 °C
3.1: sodium methylate / methanol / 20 °C
3.2: 20 °C
With
sodium methylate; trifluoroacetic anhydride;
In
tetrahydrofuran; methanol; phosphoric acid;
DOI:10.1016/j.bmc.2013.12.002