CH₂P(C₆H₅)2C[CH₂(C₃H₃N₂)]2CH₂OCH₃NiCl₂

Base Information

• Chemical Name: CH₂P(C₆H₅)2C[CH₂(C₃H₃N₂)]2CH₂OCH₃NiCl₂
• CAS No.: 623125-30-4
• Molecular Formula: C₂₄H₂₇Cl₂N₄NiOP
• Molecular Weight: 548.074
• Mol file: 623125-30-4.mol

Synonyms:

Chemical Property of CH₂P(C₆H₅)2C[CH₂(C₃H₃N₂)]2CH₂OCH₃NiCl₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of CH₂P(C₆H₅)2C[CH₂(C₃H₃N₂)]2CH₂OCH₃NiCl₂

There total 1 articles about CH₂P(C₆H₅)2C[CH₂(C₃H₃N₂)]2CH₂OCH₃NiCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

(1,2-dimethoxyethane)dichloronickel(II) (29046-78-4) + 3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether (623124-95-8) → CH2P(C6H5)2C[CH2(C3H3N2)]2CH2OCH3NiCl2 (623125-30-4)

Guidance literature:

In tetrahydrofuran; (Ar), ligand in THF added rapidly to Ni complex in THF, stirred at 25°C for 12 h; evapd.(vac.), washed (diethyl ether), dried (vac.), recrystd.(CH2Cl2/Et2O), elem. anal.;

DOI:10.1002/ejic.200200535

upstream raw materials:

(1,2-dimethoxyethane)dichloronickel(II)

3-(diphenylphosphanyl)-2,2-bis(pyrazol-1-yl-methyl) propyl methyl ether