Technology Process of C26H44B2O5P2
There total 4 articles about C26H44B2O5P2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(S,S)-1,2-bis[boranatophenyl(2-hydroxyethyl)phosphino]ethane;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
at 20 ℃;
Inert atmosphere;
Reflux;
tetraethylene glycol di(p-toluenesulfonate);
In
tetrahydrofuran; mineral oil;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/jo1024442
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: borane-THF / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere
2.1: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Inert atmosphere; Reflux
2.2: 20 °C / Inert atmosphere
With
borane-THF; sodium hydride;
In
tetrahydrofuran; mineral oil;
DOI:10.1021/jo1024442
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran; hexane; cyclohexane / 3 h / -78 °C / Inert atmosphere
1.2: 2 h / 20 °C / Inert atmosphere
1.3: Inert atmosphere
2.1: borane-THF / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere
3.1: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Inert atmosphere; Reflux
3.2: 20 °C / Inert atmosphere
With
borane-THF; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; sodium hydride;
In
tetrahydrofuran; hexane; cyclohexane; mineral oil;
DOI:10.1021/jo1024442
