diethyltin bis-(3-benzoyl-α-methylphenylacetate)

Base Information

• Chemical Name: diethyltin bis-(3-benzoyl-α-methylphenylacetate)
• CAS No.: 425376-08-5
• Molecular Formula: C₃₆H₃₆O₆Sn
• Molecular Weight: 683.388
• Mol file: 425376-08-5.mol

Synonyms:

Chemical Property of diethyltin bis-(3-benzoyl-α-methylphenylacetate)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of diethyltin bis-(3-benzoyl-α-methylphenylacetate)

There total 1 articles about diethyltin bis-(3-benzoyl-α-methylphenylacetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

ketoprofen (22071-15-4,22161-86-0) + diethyltin(IV) oxide (3682-12-0) → diethyltin bis-(3-benzoyl-α-methylphenylacetate) (425376-08-5)

Guidance literature:

In toluene; byproducts: H2O; the acid (0.02 mol) and the organotin oxide (0.01 mol) refluxed in dry toluene for 4-6 h; H2O continuously removed using Dean-Stark apparatus; toluene removed under reduced pressure; residue treated with activated charcoal in dry CHCl3; filtered; concentrated; left overnight at -5°C; elem. anal.;

DOI:10.1081/SIM-120013143

upstream raw materials:

ketoprofen

diethyltin(IV) oxide