3-Phenyltellanylpropyltellanylbenzene

Base Information

Chemical Name:3-Phenyltellanylpropyltellanylbenzene
CAS No.:105598-31-0
Molecular Formula:C15H16Te2
Molecular Weight:451.492
Hs Code.:
DSSTox Substance ID:DTXSID80572538
Nikkaji Number:J1.099.668F
Wikidata:Q82460917
Mol file:105598-31-0.mol

Synonyms:105598-31-0;DTXSID80572538;1,1'-(Propane-1,3-diylditellanyl)dibenzene

Suppliers and Price of 3-Phenyltellanylpropyltellanylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-Phenyltellanylpropyltellanylbenzene

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:6
Exact Mass:453.935884
Heavy Atom Count:17
Complexity:161

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)[Te]CCC[Te]C2=CC=CC=C2

Technology Process of 3-Phenyltellanylpropyltellanylbenzene

There total 2 articles about 3-Phenyltellanylpropyltellanylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 14683-12-6
tellurium

: 142-28-9
1,3-Dichloropropane

: 591-51-5
phenyllithium

: 105598-31-0
1,3-bis(phenyltelluro)propane

Guidance literature:: In tetrahydrofuran; THF was distilled onto Te powder under N2, frozen (-196°C), PhLi syriged in, mixt. was allowed to thaw, after Te dissolution mixt. was refrozen (-196°C), Cl(CH2)3Cl added, warmed slowly to room temp.; mixt. was hydrolyzed (satd. aq. NaCl), org. phase septd., dried, evapd. in vacuo;
DOI:10.1021/om00144a045

Reference yield:

: 14683-12-6
tellurium

: 591-51-5
phenyllithium

: 109-64-8
1,3-dibromo-propane

: 105598-31-0
1,3-bis(phenyltelluro)propane

Guidance literature:: In tetrahydrofuran; THF was distilled onto Te powder under N2, frozen (-196°C), PhLi syriged in, mixt. was allowed to thaw, after Te dissolution mixt. was refrozen (-196°C), Br(CH2)3Br added, warmed to room temp.; mixt. was hydrolyzed (satd. aq. NaCl), org. phase septd., dried, evapd. in vacuo;
DOI:10.1021/om00144a045

Reference yield: 96.0%

: 21264-30-2,90243-59-7,14592-56-4
dichloro bis(acetonitrile) palladium(II)

: 105598-31-0
1,3-bis(phenyltelluro)propane

: 118376-94-6
dichloro{meso-1,3-bis(phenyltelluro)propane}palladium(II)

: 118455-55-3
dichloro{1,3-bis(phenyltelluro)propane}palladium(II)

Guidance literature:: In dichloromethane; ligand added to a rapidly stirred soln. of complex, stirred for 3h; filtered, washed (diethyl ether), dried (vac.); elem. anal.; (meso:dl = 10:1);