C₂₉H₄₈O₆Si

Base Information

Chemical Name:C₂₉H₄₈O₆Si
CAS No.:1315594-91-2
Molecular Formula:C₂₉H₄₈O₆Si
Molecular Weight:520.782
Hs Code.:

C<sub>29</sub>H<sub>48</sub>O<sub>6</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₄₈O₆Si

Chemical Property:

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Technology Process of C₂₉H₄₈O₆Si

There total 8 articles about C₂₉H₄₈O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₃₄O₆

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1315594-91-2
C₂₉H₄₈O₆Si

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 0 ℃; for 12h; Inert atmosphere; Reflux;
DOI:10.1021/jo2010389

Reference yield:

: 1315594-73-0
C₁₂H₂₂NO₈P

: 1315594-91-2
C₂₉H₄₈O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: caesium carbonate / acetonitrile / 0.75 h / 20 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

2.1: cerium(III) chloride heptahydrate / methanol / 0.75 h / 20 °C / Inert atmosphere

2.2: 1.08 h / -78 °C / Inert atmosphere

2.3: 0 - 20 °C / Inert atmosphere

3.1: tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

4.1: potassium tri-sec-butyl-borohydride / tetrahydrofuran / 1.08 h / -78 °C / Inert atmosphere

5.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere

6.1: potassium carbonate / methanol / 1 h / 20 °C / Inert atmosphere

7.1: 1H-imidazole; dmap / dichloromethane / 12 h / 0 °C / Inert atmosphere; Reflux

With 1H-imidazole; dmap; cerium(III) chloride heptahydrate; di-isopropyl azodicarboxylate; potassium tri-sec-butyl-borohydride; potassium carbonate; caesium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; acetonitrile; 1.1: Horner-Wadsworth-Emmons olefination / 1.2: Horner-Wadsworth-Emmons olefination / 5.1: Mitsunobu reaction;
DOI:10.1021/jo2010389

Reference yield:

: 1315594-89-8
C₂₃H₃₂O₆

: 1315594-91-2
C₂₉H₄₈O₆Si

Guidance literature:: Multi-step reaction with 4 steps

1: potassium tri-sec-butyl-borohydride / tetrahydrofuran / 1.08 h / -78 °C / Inert atmosphere

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere

3: potassium carbonate / methanol / 1 h / 20 °C / Inert atmosphere

4: 1H-imidazole; dmap / dichloromethane / 12 h / 0 °C / Inert atmosphere; Reflux

With 1H-imidazole; dmap; di-isopropyl azodicarboxylate; potassium tri-sec-butyl-borohydride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; 2: Mitsunobu reaction;
DOI:10.1021/jo2010389