C₂₆H₂₅ClN₂O₆

Base Information

• Chemical Name: C₂₆H₂₅ClN₂O₆
• CAS No.: 1356844-75-1
• Molecular Formula: C₂₆H₂₅ClN₂O₆
• Molecular Weight: 496.947
• Mol file: 1356844-75-1.mol

Synonyms:

Chemical Property of C₂₆H₂₅ClN₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₅ClN₂O₆

There total 6 articles about C₂₆H₂₅ClN₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C28H29ClN2O6 → C26H25ClN2O6 (1356844-75-1)

Guidance literature:

With water; lithium hydroxide; In tetrahydrofuran; methanol; at 23 ℃; for 2h;

DOI:10.1016/j.bmcl.2011.10.123

Reference yield:

ethyl (3-hydroxy-4-methoxyphenyl)acetate → C26H25ClN2O6 (1356844-75-1)

Guidance literature:

Multi-step reaction with 5 steps

1: potassium carbonate / dimethyl sulfoxide / 8 h / 80 °C

2: palladium on activated charcoal; hydrogen / ethanol / 1 h / 20 °C

3: triethylamine / dichloromethane / 3 h / 20 °C

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 24 h / 20 °C

5: water; lithium hydroxide / tetrahydrofuran; methanol / 2 h / 23 °C

With palladium on activated charcoal; water; hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; dimethyl sulfoxide;

DOI:10.1016/j.bmcl.2011.10.123

Reference yield:

C18H17NO8 (1356844-85-3) → C26H25ClN2O6 (1356844-75-1)

Guidance literature:

Multi-step reaction with 4 steps

1: palladium on activated charcoal; hydrogen / ethanol / 1 h / 20 °C

2: triethylamine / dichloromethane / 3 h / 20 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 24 h / 20 °C

4: water; lithium hydroxide / tetrahydrofuran; methanol / 2 h / 23 °C

With palladium on activated charcoal; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane;

DOI:10.1016/j.bmcl.2011.10.123

upstream raw materials:

C₁₈H₁₇NO₈

C₁₈H₁₉NO₆

2-fluoro-5-nitrobenzoic acid