Technology Process of C26H22N2O4
There total 4 articles about C26H22N2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
piperidine;
In
methanol;
for 24h;
Inert atmosphere;
Reflux;
DOI:10.1021/jm201006x
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 8 h / 20 °C
2.1: trichlorophosphate / 0.08 h / 0 °C / Inert atmosphere
2.2: 1 h / 20 °C / Inert atmosphere
2.3: Inert atmosphere
3.1: piperidine / methanol / 24 h / Inert atmosphere; Reflux
With
piperidine; tetrabutylammomium bromide; sodium hydroxide; trichlorophosphate;
In
methanol; dichloromethane; water;
2.1: Vilsmeier-Haack formylation / 2.2: Vilsmeier-Haack formylation / 3.1: Claisen Schmidt condensation;
DOI:10.1021/jm201006x
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: boron tribromide / dichloromethane / 0.5 h / -78 - 20 °C / Inert atmosphere
1.2: Cooling with ice
2.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 8 h / 20 °C
3.1: trichlorophosphate / 0.08 h / 0 °C / Inert atmosphere
3.2: 1 h / 20 °C / Inert atmosphere
3.3: Inert atmosphere
4.1: piperidine / methanol / 24 h / Inert atmosphere; Reflux
With
piperidine; tetrabutylammomium bromide; boron tribromide; sodium hydroxide; trichlorophosphate;
In
methanol; dichloromethane; water;
3.1: Vilsmeier-Haack formylation / 3.2: Vilsmeier-Haack formylation / 4.1: Claisen Schmidt condensation;
DOI:10.1021/jm201006x
