Technology Process of C36H36F6O10
There total 5 articles about C36H36F6O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: K2Os(OH)2; methanesulfonamide; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III) / dichloromethane; water; tert-butyl alcohol / 24 h / 0 °C / Inert atmosphere
2: pyridine / 3.25 h / 0 - 20 °C / Inert atmosphere
With
methanesulfonamide; K2Os(OH)2; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III);
In
pyridine; dichloromethane; water; tert-butyl alcohol;
1: Mosher ester derivatization / 2: Mosher ester derivatization;
DOI:10.1021/ja302260d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 16 h / Inert atmosphere; Reflux
2: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / water; acetonitrile / 0.83 h / 0 - 20 °C / Inert atmosphere
3: K2Os(OH)2; methanesulfonamide; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III) / dichloromethane; water; tert-butyl alcohol / 24 h / 0 °C / Inert atmosphere
4: pyridine / 3.25 h / 0 - 20 °C / Inert atmosphere
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; methanesulfonamide; K2Os(OH)2; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; hydroquinidein 1,4-phthalazinediyl diether; lithium chloride; potassium hexacyanoferrate(III);
In
pyridine; dichloromethane; water; acetonitrile; tert-butyl alcohol;
2: Horner-Wadsworth-Emmons olefination / 3: Mosher ester derivatization / 4: Mosher ester derivatization;
DOI:10.1021/ja302260d
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydride / N,N-dimethyl-formamide / Inert atmosphere
2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 16 h / Inert atmosphere; Reflux
3: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / water; acetonitrile / 0.83 h / 0 - 20 °C / Inert atmosphere
4: K2Os(OH)2; methanesulfonamide; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III) / dichloromethane; water; tert-butyl alcohol / 24 h / 0 °C / Inert atmosphere
5: pyridine / 3.25 h / 0 - 20 °C / Inert atmosphere
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; methanesulfonamide; K2Os(OH)2; sodium hydride; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; hydroquinidein 1,4-phthalazinediyl diether; lithium chloride; potassium hexacyanoferrate(III);
In
pyridine; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
3: Horner-Wadsworth-Emmons olefination / 4: Mosher ester derivatization / 5: Mosher ester derivatization;
DOI:10.1021/ja302260d