C₁₇H₁₈N₂O₄S₂*ClH

Base Information

Chemical Name:C₁₇H₁₈N₂O₄S₂*ClH
CAS No.:1333481-64-3
Molecular Formula:C₁₇H₁₈N₂O₄S₂*ClH
Molecular Weight:414.934
Hs Code.:

C<sub>17</sub>H<sub>18</sub>N<sub>2</sub>O<sub>4</sub>S<sub>2</sub>*ClH

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₈N₂O₄S₂*ClH

Chemical Property:

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Technology Process of C₁₇H₁₈N₂O₄S₂*ClH

There total 9 articles about C₁₇H₁₈N₂O₄S₂*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1333379-34-2
C₂₂H₂₆N₂O₆S₂

: 1333481-64-3
C₁₇H₁₈N₂O₄S₂*ClH

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; ethyl acetate; at 0 - 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/jm200566e

Reference yield:

: 869577-67-3
C₁₅H₁₅NOS

: 1333481-64-3
C₁₇H₁₈N₂O₄S₂*ClH

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / methanol / 2 h / 60 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 72 h / Inert atmosphere; Cooling with ice

3: thiourea / methanol; dichloromethane / 18 h / 20 °C / Inert atmosphere

4: hydrogenchloride / 1,4-dioxane; dichloromethane; ethyl acetate / 48 h / 0 - 20 °C / Inert atmosphere

5: 4-methyl-morpholine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere; Cooling

6: hydrogenchloride / 1,4-dioxane; dichloromethane; ethyl acetate / 48 h / 0 - 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; triethylamine; thiourea; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm200566e

Reference yield:

: 1333481-74-5
tert-butyl (4-(4-((oxiran-2-ylmethyl)sulfonyl)phenoxy)phenyl)carbamate

: 1333481-64-3
C₁₇H₁₈N₂O₄S₂*ClH

Guidance literature:: Multi-step reaction with 4 steps

1: thiourea / methanol; dichloromethane / 18 h / 20 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane; dichloromethane; ethyl acetate / 48 h / 0 - 20 °C / Inert atmosphere

3: 4-methyl-morpholine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere; Cooling

4: hydrogenchloride / 1,4-dioxane; dichloromethane; ethyl acetate / 48 h / 0 - 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; thiourea; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm200566e