Technology Process of dodecyl (S)-2-(4-Hydroxy-3,5-diiodobenzamido)propanoate
There total 2 articles about dodecyl (S)-2-(4-Hydroxy-3,5-diiodobenzamido)propanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
L-alanine dodecyl ester trifluoroacetate;
With
triethylamine;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
3,5-diiodo-4-hydroxybenzoic acid;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1021/ma401730e
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0 - 20 °C
2.1: trifluoroacetic acid / tetrahydrofuran / 0 - 20 °C
3.1: triethylamine / tetrahydrofuran / 2 h / 20 °C
3.2: TRIAZIMOCH / 20 °C
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ma401730e
