bis(tetrahydrofurane)tris(triphenylsilanolato)vanadium(III)

Base Information

Chemical Name:bis(tetrahydrofurane)tris(triphenylsilanolato)vanadium(III)
CAS No.:220260-82-2
Molecular Formula:C₆₂H₆₁O₅Si₃V
Molecular Weight:1021.36
Hs Code.:

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Chemical Property of bis(tetrahydrofurane)tris(triphenylsilanolato)vanadium(III)

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Technology Process of bis(tetrahydrofurane)tris(triphenylsilanolato)vanadium(III)

There total 1 articles about bis(tetrahydrofurane)tris(triphenylsilanolato)vanadium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 131063-11-1,16997-51-6,19559-06-9
Vanadium (III) chloride-(tris-tetrahydrofuran)

: 2004-11-7
triphenylsilanol lithium salt

: 220260-82-2
bis(tetrahydrofurane)tris(triphenylsilanolato)vanadium(III)

: 18822-50-9
tris-(triphenylsiloxy)-vanadium oxide

Guidance literature:: In tetrahydrofuran; byproducts: LiCl; under Ar, THF soln. of V-compd. and 3 equiv. of Li-compd. were mixed, stirring for 24 h; soln. was evapd. in vac., residue was taken in toluene, LiCl was centrifuged off, soln. was cooled to -18 °C, two types of crystals were sepd. with several times washing with n-pentane, recrystn. twice from toluene, drying in vac., elem. anal.;
DOI:10.1515/znb-2002-0702

Reference yield: 97.0%

: 220260-82-2
bis(tetrahydrofurane)tris(triphenylsilanolato)vanadium(III)

: 461643-88-9
(tetrahydrofurane)tris(triphenylsilanolato)vanadium(III)

Guidance literature:: In neat (no solvent); byproducts: THF; heating under stirring in vac. (1E-6 Torr) at 110 °C for 2 h; elem. anal.;
DOI:10.1515/znb-2002-0702

Reference yield: 79.0%

: 110-86-1
pyridine

: 220260-82-2
bis(tetrahydrofurane)tris(triphenylsilanolato)vanadium(III)

: 108-88-3,15644-74-3,16713-13-6
toluene

: bis(pyridine)tris(triphenylsilanolato)vanadium(III)*toluene

Guidance literature:: In pyridine; stirring at room temp. for 24 h, under Ar; solvent was removed, residue was recrystd. from toluene/n-hexane (9:1);
DOI:10.1515/znb-2002-0702