bis(triphenylphosphine)monoacetonitrile tricarbonylmolybdenum

Base Information

Chemical Name:bis(triphenylphosphine)monoacetonitrile tricarbonylmolybdenum
CAS No.:82916-66-3
Molecular Formula:C₄₁H₃₃MoNO₃P₂
Molecular Weight:745.605
Hs Code.:

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Chemical Property of bis(triphenylphosphine)monoacetonitrile tricarbonylmolybdenum

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Technology Process of bis(triphenylphosphine)monoacetonitrile tricarbonylmolybdenum

There total 3 articles about bis(triphenylphosphine)monoacetonitrile tricarbonylmolybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 15038-48-9,17731-95-2
tris(acetonitrile)tricarbonylmolybdenum⁽⁰⁾

: 603-35-0
triphenylphosphine

: 31265-07-3,31265-08-4,82916-66-3
fac-(CO)3(PPh₃)2Mo(NCMe)

Guidance literature:: In acetonitrile; (N2); PPh3 was added to soln. of molibdenium complex in MeCN at 80°C, refluxed for 12 h; filtered, washed with MeCN, dried in vac., elem. anal.;
DOI:10.1016/j.jorganchem.2009.06.042

Reference yield: 20.0%

: 54460-81-0,83057-97-0
fac-(acetonitrile)2triphenylphosphinetricarbonylmolybdenum

: 50400-06-1
8-azidoquinoline

: 135740-68-0
cis-triphenylphosphinimine(azidoquinoline) tetracarbonylmolybdenum(O)*monoacetonitrile

: 31265-07-3,31265-08-4,82916-66-3
bis(triphenylphosphine)monoacetonitrile tricarbonylmolybdenum

: 135740-69-1
triphenylphosphine((triphenylphosphinimine)quinoline)tricarbonylmolybdenum

Guidance literature:: With CO; In acetonitrile; byproducts: CH3CN; Addn. of Mo-compd. in CH3CN soln. to 8-azidoquinoline at -5°C, soln. was stirred at -5°C for 1 h (N2).; React. is monitored by IR, isolation at room temp., elem. anal.;