C₆₅H₄₈N₂

Base Information

Chemical Name:C₆₅H₄₈N₂
CAS No.:1265177-22-7
Molecular Formula:C₆₅H₄₈N₂
Molecular Weight:857.11
Hs Code.:

C<sub>65</sub>H<sub>48</sub>N<sub>2</sub>

Synonyms:

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Chemical Property of C₆₅H₄₈N₂

Chemical Property:

Purity/Quality:

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Technology Process of C₆₅H₄₈N₂

There total 9 articles about C₆₅H₄₈N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92-66-0
4-bromo-1,1'-biphenyl

: 1265177-22-7
C₆₅H₄₈N₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 3 h / 90 °C

2.1: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 3 h / 90 °C

3.1: n-butyllithium / hexane; tetrahydrofuran / -78 - -30 °C / Inert atmosphere

3.2: 2 h / -78 - 20 °C / Inert atmosphere

3.3: 0.5 h

4.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 5 h / 80 °C

5.1: sodium t-butanolate / palladium diacetate; XPhos / toluene / 3 h / 90 °C

6.1: toluene-4-sulfonic acid / toluene; ethanol / 24 h / 110 °C

7.1: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 3 h / 90 °C

With n-butyllithium; potassium carbonate; toluene-4-sulfonic acid; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium diacetate; XPhos; In tetrahydrofuran; ethanol; hexane; water; toluene;

Reference yield:

: 92-67-1
4-phenylalanine

: 1265177-22-7
C₆₅H₄₈N₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 3 h / 90 °C

2.1: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 3 h / 90 °C

3.1: n-butyllithium / hexane; tetrahydrofuran / -78 - -30 °C / Inert atmosphere

3.2: 2 h / -78 - 20 °C / Inert atmosphere

3.3: 0.5 h

4.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 5 h / 80 °C

5.1: sodium t-butanolate / palladium diacetate; XPhos / toluene / 3 h / 90 °C

6.1: toluene-4-sulfonic acid / toluene; ethanol / 24 h / 110 °C

7.1: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 3 h / 90 °C

With n-butyllithium; potassium carbonate; toluene-4-sulfonic acid; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium diacetate; XPhos; In tetrahydrofuran; ethanol; hexane; water; toluene;

Reference yield:

: 499128-71-1
N-([1′,1′-biphenyl]-4-yl)-N-(4-bromophenyl)-[1,1′-biphenyl]-4-amine

: 1265177-22-7
C₆₅H₄₈N₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / -78 - -30 °C / Inert atmosphere

1.2: 2 h / -78 - 20 °C / Inert atmosphere

1.3: 0.5 h

2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 5 h / 80 °C

3.1: sodium t-butanolate / palladium diacetate; XPhos / toluene / 3 h / 90 °C

4.1: toluene-4-sulfonic acid / toluene; ethanol / 24 h / 110 °C

5.1: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 3 h / 90 °C

With n-butyllithium; potassium carbonate; toluene-4-sulfonic acid; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium diacetate; XPhos; In tetrahydrofuran; ethanol; hexane; water; toluene;