C₄₈H₄₅N₇O₂

Base Information

• Chemical Name: C₄₈H₄₅N₇O₂
• CAS No.: 1333325-10-2
• Molecular Formula: C₄₈H₄₅N₇O₂
• Molecular Weight: 751.931
• Mol file: 1333325-10-2.mol

Synonyms:

Chemical Property of C₄₈H₄₅N₇O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₈H₄₅N₇O₂

There total 1 articles about C₄₈H₄₅N₇O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2,6-dibromophenylazo)pyrrolidine (338730-94-2) + C22H26N2OSn (1333325-09-9) → C48H45N7O2 (1333325-10-2)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; for 48h; Inert atmosphere; Reflux;

DOI:10.1039/c1cc11209k

Reference yield:

C48H45N7O2 (1333325-10-2) → C42H33IN4O2

Guidance literature:

Multi-step reaction with 2 steps

1: iodine / dichloromethane / 20 h / Inert atmosphere; Reflux

2: hydrogen iodide / water / 20 h / 120 °C / Inert atmosphere

With hydrogen iodide; iodine; In dichloromethane; water;

DOI:10.1039/c1cc11209k

Reference yield:

C48H45N7O2 (1333325-10-2) → C60H74N4O2Si2 (1333325-17-9)

Guidance literature:

Multi-step reaction with 4 steps

1: iodine / dichloromethane / 20 h / Inert atmosphere; Reflux

2: hydrogen iodide / water / 20 h / 120 °C / Inert atmosphere

3: triethylamine / dichloromethane / 18 h / -78 - 20 °C / Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / toluene / 16 h / 10 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen iodide; iodine; triethylamine; In dichloromethane; water; toluene; 4: Sonogashira coupling;

DOI:10.1039/c1cc11209k

upstream raw materials:

1-(2,6-dibromophenylazo)pyrrolidine

C₂₂H₂₆N₂OSn

Downstream raw materials:

C₆₀H₇₄N₄O₂Si₂

C₅₂H₄₆N₄O₂

C₄₄H₃₇IN₄O₂

C₆₀H₇₃IN₄O₂Si₂