Cd₂(N-(1-pyridin-2-ylbenzylidene)-N-[2-(4-(2-[(1-pyridin-2-ylbenzylidene)amino]ethyl)piperazin-1-yl)ethyl]amine)(H₂O)2(N₃)4

Base Information

• Chemical Name: Cd₂(N-(1-pyridin-2-ylbenzylidene)-N-[2-(4-(2-[(1-pyridin-2-ylbenzylidene)amino]ethyl)piperazin-1-yl)ethyl]amine)(H₂O)2(N₃)4
• CAS No.: 959850-45-4
• Molecular Formula: C₃₂H₃₈Cd₂N₁₈O₂
• Molecular Weight: 931.593
• Mol file: 959850-45-4.mol

Synonyms:

Chemical Property of Cd₂(N-(1-pyridin-2-ylbenzylidene)-N-[2-(4-(2-[(1-pyridin-2-ylbenzylidene)amino]ethyl)piperazin-1-yl)ethyl]amine)(H₂O)2(N₃)4

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cd₂(N-(1-pyridin-2-ylbenzylidene)-N-[2-(4-(2-[(1-pyridin-2-ylbenzylidene)amino]ethyl)piperazin-1-yl)ethyl]amine)(H₂O)2(N₃)4

There total 1 articles about Cd₂(N-(1-pyridin-2-ylbenzylidene)-N-[2-(4-(2-[(1-pyridin-2-ylbenzylidene)amino]ethyl)piperazin-1-yl)ethyl]amine)(H₂O)2(N₃)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

sodium azide + cadmium(II) perchlorate hexahydrate + N-((1-pyridin-2-yl)benzylidene)-N'-[2-(4-[2-[((1-pyridin-2-yl)benzylidene)amino]ethyl]piperazin-1-yl)-ethyl]amine (959850-48-7) → Cd2(N-(1-pyridin-2-ylbenzylidene)-N-[2-(4-(2-[(1-pyridin-2-ylbenzylidene)amino]ethyl)piperazin-1-yl)ethyl]amine)(H2O)2(N3)4 (959850-45-4)

Guidance literature:

In methanol; acetonitrile; byproducts: NaClO4, H2O; 0.5 equiv. of MeOH soln. of N-compd. was added to MeCN soln. of Cd-complex with stirring, 2 equiv. of MeOH soln. of NaN3 was added, 298 K; soln. was filtered, kept to slowly evaporate for 7 days, crystals were sepd., washed with toluene, dried in vac. over silica gel, elem. anal.;

DOI:10.1016/j.poly.2007.07.029

upstream raw materials:

N-((1-pyridin-2-yl)benzylidene)-N'-[2-(4-[2-[((1-pyridin-2-yl)benzylidene)amino]ethyl]piperazin-1-yl)-ethyl]amine

Refernces