diamminesilver(I) bis(2-amino-5-nitrobenzoato-κ2O1,O1')silver(I)

Base Information

• Chemical Name: diamminesilver(I) bis(2-amino-5-nitrobenzoato-κ2O1,O1')silver(I)
• CAS No.: 1311134-32-3
• Molecular Formula: AgH₆N₂*C₁₄H₁₀AgN₄O₈
• Molecular Weight: 612.053
• Mol file: 1311134-32-3.mol

Synonyms:

Chemical Property of diamminesilver(I) bis(2-amino-5-nitrobenzoato-κ2O1,O1')silver(I)

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of diamminesilver(I) bis(2-amino-5-nitrobenzoato-κ2O1,O1')silver(I)

There total 1 articles about diamminesilver(I) bis(2-amino-5-nitrobenzoato-κ2O1,O1')silver(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

ammonia (7664-41-7) + 2-amino-5-nitro-benzoic acid (616-79-5) + silver(l) oxide (20667-12-3) → diamminesilver(I) bis(2-amino-5-nitrobenzoato-κ2O1,O1')silver(I) (1311134-32-3)

Guidance literature:

In methanol; water; Sonication; mixt. of Ag2O (0.5 mmol) and C6H3(NH2)(NO2)COOH (1 mmol) stirred in MeOH/H2O (1:1 v/v), aq. NH3 added dropwise under ultrasonic treatment; evapd. slowly at room temp. in the dark for several d, washed with EtOH and Et2O; elem. anal.;

DOI:10.1107/S0108270110020585

upstream raw materials:

ammonia

2-amino-5-nitro-benzoic acid

silver(l) oxide