Technology Process of C42H57N3O8Si
There total 6 articles about C42H57N3O8Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C21H39N3O8Si;
With
tetra-(n-butyl)ammonium iodide; sodium hydride;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 0.166667h;
benzyl bromide;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 2h;
DOI:10.1002/chem.201204550
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium methylate / dichloromethane; methanol / 0.5 h / 20 °C
1.2: IR-120 resin
2.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C
2.2: 2 h / 0 - 20 °C
With
sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201204550
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Molecular sieve
2.1: trifluoroacetic acid; trifluoroacetic anhydride / dichloromethane / 0.5 h / 0 °C
3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0 °C / Molecular sieve; Inert atmosphere
4.1: sodium methylate / dichloromethane; methanol / 0.5 h / 20 °C
4.2: IR-120 resin
5.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C
5.2: 2 h / 0 - 20 °C
With
2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; trifluoroacetic acid; trifluoroacetic anhydride;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201204550
