bis(2-cyclobutyl-4-phenyl-1H-inden-1-yl)dimethylsilane

Base Information

Chemical Name:bis(2-cyclobutyl-4-phenyl-1H-inden-1-yl)dimethylsilane
CAS No.:1217864-56-6
Molecular Formula:C₄₀H₄₀Si
Molecular Weight:548.843
Hs Code.:

Synonyms:

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Chemical Property of bis(2-cyclobutyl-4-phenyl-1H-inden-1-yl)dimethylsilane

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Technology Process of bis(2-cyclobutyl-4-phenyl-1H-inden-1-yl)dimethylsilane

There total 8 articles about bis(2-cyclobutyl-4-phenyl-1H-inden-1-yl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₁₉BrO₂

: 1217864-56-6
bis(2-cyclobutyl-4-phenyl-1H-inden-1-yl)dimethylsilane

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hydroxide / methanol; water / 10 h / Reflux; Inert atmosphere

2.1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C / Reflux; Inert atmosphere

3.1: aluminum (III) chloride / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: palladium diacetate; sodium carbonate; triphenylphosphine / 1,2-dimethoxyethane; water / 8 h / Reflux; Inert atmosphere

5.1: lithium aluminium tetrahydride / diethyl ether / -40 - 20 °C / Inert atmosphere

6.1: toluene-4-sulfonic acid / benzene / 2 h / Inert atmosphere; Reflux

7.1: n-butyllithium / diethyl ether; hexane / -40 - 20 °C / Inert atmosphere

7.2: 16 h / 20 °C / Inert atmosphere

With aluminum (III) chloride; lithium aluminium tetrahydride; n-butyllithium; thionyl chloride; palladium diacetate; sodium carbonate; toluene-4-sulfonic acid; N,N-dimethyl-formamide; triphenylphosphine; potassium hydroxide; In methanol; 1,2-dimethoxyethane; diethyl ether; hexane; dichloromethane; water; benzene; 3.1: Friedel-Crafts reaction / 4.1: Suzuki coupling;
DOI:10.1007/s11172-008-0217-2

Reference yield:

: C₁₃H₁₄BrClO

: 1217864-56-6
bis(2-cyclobutyl-4-phenyl-1H-inden-1-yl)dimethylsilane

Guidance literature:: Multi-step reaction with 5 steps

1.1: aluminum (III) chloride / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: palladium diacetate; sodium carbonate; triphenylphosphine / 1,2-dimethoxyethane; water / 8 h / Reflux; Inert atmosphere

3.1: lithium aluminium tetrahydride / diethyl ether / -40 - 20 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / benzene / 2 h / Inert atmosphere; Reflux

5.1: n-butyllithium / diethyl ether; hexane / -40 - 20 °C / Inert atmosphere

5.2: 16 h / 20 °C / Inert atmosphere

With aluminum (III) chloride; lithium aluminium tetrahydride; n-butyllithium; palladium diacetate; sodium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In 1,2-dimethoxyethane; diethyl ether; hexane; dichloromethane; water; benzene; 1.1: Friedel-Crafts reaction / 2.1: Suzuki coupling;
DOI:10.1007/s11172-008-0217-2

Reference yield:

: 1217864-50-0
3-(2-bromophenyl)-2-cyclobutylpropionic acid

: 1217864-56-6
bis(2-cyclobutyl-4-phenyl-1H-inden-1-yl)dimethylsilane

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C / Reflux; Inert atmosphere

2.1: aluminum (III) chloride / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: palladium diacetate; sodium carbonate; triphenylphosphine / 1,2-dimethoxyethane; water / 8 h / Reflux; Inert atmosphere

4.1: lithium aluminium tetrahydride / diethyl ether / -40 - 20 °C / Inert atmosphere

5.1: toluene-4-sulfonic acid / benzene / 2 h / Inert atmosphere; Reflux

6.1: n-butyllithium / diethyl ether; hexane / -40 - 20 °C / Inert atmosphere

6.2: 16 h / 20 °C / Inert atmosphere

With aluminum (III) chloride; lithium aluminium tetrahydride; n-butyllithium; thionyl chloride; palladium diacetate; sodium carbonate; toluene-4-sulfonic acid; N,N-dimethyl-formamide; triphenylphosphine; In 1,2-dimethoxyethane; diethyl ether; hexane; dichloromethane; water; benzene; 2.1: Friedel-Crafts reaction / 3.1: Suzuki coupling;
DOI:10.1007/s11172-008-0217-2