1--cyclohexan-1-ol

Base Information

• Chemical Name: 1--cyclohexan-1-ol
• CAS No.: 1848-15-3
• Molecular Formula: C₁₄H₂₀O₃
• Molecular Weight: 236.311
• Mol file: 1848-15-3.mol

Synonyms:

Chemical Property of 1--cyclohexan-1-ol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1--cyclohexan-1-ol

There total 1 articles about 1--cyclohexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + 1,4-dimethoxybezene (150-78-7) → 1--cyclohexan-1-ol (1848-15-3)

Guidance literature:

Multistep reaction; (i) PhLi, (ii) /BRN= 385735/, (heating);

DOI:10.1039/jr9650001495

Reference yield:

1--cyclohexan-1-ol (1848-15-3) → 1-(2,5-dimethoxyphenyl)cyclohexene (1848-14-2)

Guidance literature:

With oxalic acid; In toluene; Heating;

DOI:10.1039/jr9650001495

Reference yield:

1--cyclohexan-1-ol (1848-15-3) → <2-(p-Dimethoxy-phenyl)-3-oxo-cyclohexyl>-essigsaeure

Guidance literature:

Multi-step reaction with 4 steps

1: oxalic acid / toluene / Heating

2: (i) pentyl nitrite, aq. HCl, AcOH, (ii) Py

3: aq. H₂SO₄ / Heating

4: (i) KOtBu, (ii) aq. HCl, AcOH, (heating), (iii) (decarboxylation)

With sulfuric acid; oxalic acid; In toluene;

DOI:10.1039/jr9650001495

upstream raw materials:

cyclohexanone

1,4-dimethoxybezene

Downstream raw materials:

1-(2,5-dimethoxyphenyl)cyclohexene

2-(2',5'-dimethoxyphenyl)cyclohex-2-enone

2-(p-Dimethoxy-phenyl)-cyclohex-2-en-1-on-oxim