C₁₇H₁₈O₄

Base Information

• Chemical Name: C₁₇H₁₈O₄
• CAS No.: 157435-12-6
• Molecular Formula: C₁₇H₁₈O₄
• Molecular Weight: 286.328
• Mol file: 157435-12-6.mol

Synonyms:

Chemical Property of C₁₇H₁₈O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₈O₄

There total 1 articles about C₁₇H₁₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-Methyl lactate (27871-49-4,2155-30-8) + 4-Benzyloxyphenol (103-16-2) → C17H18O4 (157435-12-6)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In dichloromethane; at 0 ℃;

DOI:10.1080/15421406.2012.674466

Reference yield:

C17H18O4 (157435-12-6) → C32H29F17O6 (1412900-14-1)

Guidance literature:

Multi-step reaction with 4 steps

1: water; sodium hydroxide / ethanol

2: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 0 - 20 °C

3: palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

4: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 48 h / 0 - 20 °C / Inert atmosphere

With dmap; palladium on activated charcoal; water; hydrogen; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; ethanol; ethyl acetate;

DOI:10.1080/15421406.2012.674466

Reference yield:

C17H18O4 (157435-12-6) → C33H31F17O6 (1412900-15-2)

Guidance literature:

Multi-step reaction with 4 steps

1: water; sodium hydroxide / ethanol

2: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 0 - 20 °C

3: palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

4: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 48 h / 0 - 20 °C / Inert atmosphere

With dmap; palladium on activated charcoal; water; hydrogen; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; ethanol; ethyl acetate;

DOI:10.1080/15421406.2012.674466

upstream raw materials:

(S)-Methyl lactate

4-Benzyloxyphenol

Downstream raw materials:

(R)-(+)-2-[4-(benzyloxy)phenyloxy]propionic acid

C₃₀H₂₅F₁₇O₆

C₃₁H₂₇F₁₇O₆

C₃₂H₂₉F₁₇O₆