2,4-N,N-trifluorophenyl-1,3-tetramesitylcyclogermazane

Base Information

Chemical Name:2,4-N,N-trifluorophenyl-1,3-tetramesitylcyclogermazane
CAS No.:169053-38-7
Molecular Formula:C₄₈H₄₈F₆Ge₂N₂
Molecular Weight:912.093
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-N,N-trifluorophenyl-1,3-tetramesitylcyclogermazane

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Technology Process of 2,4-N,N-trifluorophenyl-1,3-tetramesitylcyclogermazane

There total 4 articles about 2,4-N,N-trifluorophenyl-1,3-tetramesitylcyclogermazane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: N-dimesitylfluoroogermyl N-2,4,6-trifluoroanilinolithium *3THF

: 169053-38-7
2,4-N,N-trifluorophenyl-1,3-tetramesitylcyclogermazane

Guidance literature:: In benzene; byproducts: LiF; N2 or Ar; sample soln. heating at 40. for 3 h,stirring for 1 h at 20°C, soln. concn. under reduced pressure; residue treatment with pentane;
DOI:10.1080/10426509608046364

Reference yield:

: N-dimesitylfluoroogermyl N-2,4,6-trifluoroanilinolithium *3THF

: 7789-48-2
magnesium bromide

: 132775-06-5
2,2,4,4-tetramesityl-1,3,2,4-dioxadigermetane

: 169053-38-7
2,4-N,N-trifluorophenyl-1,3-tetramesitylcyclogermazane

Guidance literature:: With N-tert-butyl phenylnitrone; In tetrahydrofuran; benzene; N2 or Ar; MgBr2 soln. (THF) addn. at -80°C to Ge-compd., after 30h at 20°C org. reagent soln. (C6H6) addn., after 24 h at 20.degr ee.C and 4 d at 80°C centrifugation and soln. concn.;
DOI:10.1080/10426509608046364