C₁₈H₂₆O

Base Information

Chemical Name:C₁₈H₂₆O
CAS No.:1384112-66-6
Molecular Formula:C₁₈H₂₆O
Molecular Weight:258.404
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₂₆O

Chemical Property:

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Technology Process of C₁₈H₂₆O

There total 5 articles about C₁₈H₂₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₄O₂

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1384112-66-6
C₁₈H₂₆O

Guidance literature:: With potassium tert-butylate; In toluene; at 20 - 110 ℃;
DOI:10.1016/j.bmcl.2012.05.022

Reference yield:

: 1384112-62-2
C₁₈H₂₉NO₂

: 1384112-66-6
C₁₈H₂₆O

Guidance literature:: Multi-step reaction with 8 steps

1: boron tribromide / dichloromethane / -78 - 0 °C

2: pyridine / dichloromethane / 0 °C

3: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; lithium chloride / N,N-dimethyl-formamide / 100 °C

4: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol

5: boron trifluoride diethyl etherate / dichloromethane / -78 - 0 °C

6: toluene-4-sulfonic acid / toluene / 110 °C

7: diisobutylaluminium hydride / dichloromethane / -78 °C

8: potassium tert-butylate / toluene / 20 - 110 °C

With pyridine; bis-triphenylphosphine-palladium(II) chloride; sodium periodate; osmium(VIII) oxide; boron trifluoride diethyl etherate; potassium tert-butylate; boron tribromide; diisobutylaluminium hydride; toluene-4-sulfonic acid; triphenylphosphine; lithium chloride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 3: Stille coupling / 4: Lemieux-Johnson oxidation;
DOI:10.1016/j.bmcl.2012.05.022

Reference yield:

: C₁₈H₂₇NO₂

: 1384112-66-6
C₁₈H₂₆O

Guidance literature:: Multi-step reaction with 9 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C

2: boron tribromide / dichloromethane / -78 - 0 °C

3: pyridine / dichloromethane / 0 °C

4: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; lithium chloride / N,N-dimethyl-formamide / 100 °C

5: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol

6: boron trifluoride diethyl etherate / dichloromethane / -78 - 0 °C

7: toluene-4-sulfonic acid / toluene / 110 °C

8: diisobutylaluminium hydride / dichloromethane / -78 °C

9: potassium tert-butylate / toluene / 20 - 110 °C

With pyridine; bis-triphenylphosphine-palladium(II) chloride; sodium periodate; osmium(VIII) oxide; palladium 10% on activated carbon; boron trifluoride diethyl etherate; potassium tert-butylate; hydrogen; boron tribromide; diisobutylaluminium hydride; toluene-4-sulfonic acid; triphenylphosphine; lithium chloride; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 4: Stille coupling / 5: Lemieux-Johnson oxidation;
DOI:10.1016/j.bmcl.2012.05.022