Technology Process of (3aR,4S,6aS)-6a-Benzo[1,3]dioxol-5-yl-5-benzoyl-2-oxo-hexahydro-furo[2,3-c]pyrrole-4-carboxylic acid
There total 9 articles about (3aR,4S,6aS)-6a-Benzo[1,3]dioxol-5-yl-5-benzoyl-2-oxo-hexahydro-furo[2,3-c]pyrrole-4-carboxylic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: CeCl3 / tetrahydrofuran; diethyl ether
2: trifluoroacetic acid
With
cerium(III) chloride; trifluoroacetic acid;
In
tetrahydrofuran; diethyl ether;
DOI:10.1016/0040-4039(94)88105-7
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 89 percent / 1 N NaOH / diethyl ether
2: 82 percent / benzene; various solvent(s) / Heating
3: 97 percent / NaIO4, RuO2*H2O / H2O; CCl4; CHCl3
4: molsieves 5 A / benzene
5: 1.) K2CO3 / 1.) CH3CN; 2.) H2O, CH3CO2H
6: CeCl3 / tetrahydrofuran; diethyl ether
7: trifluoroacetic acid
With
ruthenium(IV) oxide; sodium hydroxide; sodium periodate; cerium(III) chloride; 5A molecular sieve; potassium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; tetrachloromethane; diethyl ether; chloroform; water; benzene;
DOI:10.1016/0040-4039(94)88105-7
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 82 percent / benzene; various solvent(s) / Heating
2: 97 percent / NaIO4, RuO2*H2O / H2O; CCl4; CHCl3
3: molsieves 5 A / benzene
4: 1.) K2CO3 / 1.) CH3CN; 2.) H2O, CH3CO2H
5: CeCl3 / tetrahydrofuran; diethyl ether
6: trifluoroacetic acid
With
ruthenium(IV) oxide; sodium periodate; cerium(III) chloride; 5A molecular sieve; potassium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; tetrachloromethane; diethyl ether; chloroform; water; benzene;
DOI:10.1016/0040-4039(94)88105-7
