2-Furancarboxylic acid, tetrahydro-5-oxo-2-[3-oxo-4-[(phenylacetyl)amino]-2-isoxazolidinyl]-, monosodium salt

Base Information

Chemical Name:2-Furancarboxylic acid, tetrahydro-5-oxo-2-[3-oxo-4-[(phenylacetyl)amino]-2-isoxazolidinyl]-, monosodium salt
CAS No.:105629-12-7
Molecular Formula:C₁₆H₁₅N₂O₇*Na
Molecular Weight:370.294
Hs Code.:
Mol file:105629-12-7.mol

Synonyms:

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Chemical Property of 2-Furancarboxylic acid, tetrahydro-5-oxo-2-[3-oxo-4-[(phenylacetyl)amino]-2-isoxazolidinyl]-, monosodium salt

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Technology Process of 2-Furancarboxylic acid, tetrahydro-5-oxo-2-[3-oxo-4-[(phenylacetyl)amino]-2-isoxazolidinyl]-, monosodium salt

There total 8 articles about 2-Furancarboxylic acid, tetrahydro-5-oxo-2-[3-oxo-4-[(phenylacetyl)amino]-2-isoxazolidinyl]-, monosodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106944-93-8,106963-77-3
5-Oxo-2-((S)-3-oxo-4-phenylacetylamino-isoxazolidin-2-yl)-tetrahydro-furan-2-carboxylic acid benzhydryl ester

: 105629-12-7,106944-92-7,106963-76-2,113194-95-9,113194-96-0
Na salt of N-phenylacetyl-4-amino-lactivinic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 0.833333h; Yield given; Ambient temperature; 0.1m phosphate buffer, pH= 7.5;
DOI:10.1016/S0040-4020(01)90098-5

Reference yield:

: 106962-17-8,106962-18-9,115441-24-2
benzhydryl 2-<(4S)-4-amino-3-oxo-2-isoxazolidinyl>-5-oxo-2-tetrahydrofurancarboxylate

: 105629-12-7,106944-92-7,106963-76-2,113194-95-9,113194-96-0
Na salt of N-phenylacetyl-4-amino-lactivinic acid

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethylacetamide / CH₂Cl₂ / 0.5 h / 0 °C

2: H₂ / 10percent Pd-C / tetrahydrofuran / 0.83 h / Ambient temperature; 0.1m phosphate buffer, pH= 7.5

With N,N-dimethyl acetamide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)90098-5

Reference yield:

: 103-80-0
phenylacetyl chloride

: 105629-12-7,106944-92-7,106963-76-2,113194-95-9,113194-96-0
Na salt of N-phenylacetyl-4-amino-lactivinic acid

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethylacetamide / CH₂Cl₂ / 0.5 h / 0 °C

2: H₂ / 10percent Pd-C / tetrahydrofuran / 0.83 h / Ambient temperature; 0.1m phosphate buffer, pH= 7.5

With N,N-dimethyl acetamide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)90098-5