[cis-bis[glyoxalbis(cyclohexylimine)-N,N']][1,2,3,4-tetrakis(methoxycarbonyl)-1,3-butadien-1,4-diyl]iron

Base Information

Chemical Name:[cis-bis[glyoxalbis(cyclohexylimine)-N,N']][1,2,3,4-tetrakis(methoxycarbonyl)-1,3-butadien-1,4-diyl]iron
CAS No.:101808-21-3
Molecular Formula:C₄₀H₆₀FeN₄O₈
Molecular Weight:780.785
Hs Code.:

Synonyms:

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Chemical Property of [cis-bis[glyoxalbis(cyclohexylimine)-N,N']][1,2,3,4-tetrakis(methoxycarbonyl)-1,3-butadien-1,4-diyl]iron

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Technology Process of [cis-bis[glyoxalbis(cyclohexylimine)-N,N']][1,2,3,4-tetrakis(methoxycarbonyl)-1,3-butadien-1,4-diyl]iron

There total 2 articles about [cis-bis[glyoxalbis(cyclohexylimine)-N,N']][1,2,3,4-tetrakis(methoxycarbonyl)-1,3-butadien-1,4-diyl]iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 62801-14-3
bis[glyoxalbis(cyclohexylimine)]iron

: 762-42-5
dimethyl acetylenedicarboxylate

: 101808-21-3
[cis-bis[glyoxalbis(cyclohexylimine)-N,N']][1,2,3,4-tetrakis(methoxycarbonyl)-1,3-butadien-1,4-diyl]iron

Guidance literature:: In tetrahydrofuran; addn. of the ester-compd. to a soln. of the Fe(0)-complex (room temp., inert gas atmosphere), colour change of soln. from brown to deep blue, stirring for 2 h; removal of volatiles in vac., residue is redissolved (hot MeOH), then cooled, crystals are obtained, filtration, elem. anal.;

Reference yield:

: N,N'-di-cyclohexyl-1,4-diazabuta-1,3-diene

: 101808-21-3
[cis-bis[glyoxalbis(cyclohexylimine)-N,N']][1,2,3,4-tetrakis(methoxycarbonyl)-1,3-butadien-1,4-diyl]iron

Guidance literature:: Multi-step reaction with 2 steps

1: Na / diethyl ether

2: tetrahydrofuran

With Na; In tetrahydrofuran; diethyl ether;