2'-Chloro-2,4-dioxo-1,3-dimethyl-6'-phenyl-1,2,3,4-tetrahydro-4',5-dipyrimidinyl

Base Information

Chemical Name:2'-Chloro-2,4-dioxo-1,3-dimethyl-6'-phenyl-1,2,3,4-tetrahydro-4',5-dipyrimidinyl
CAS No.:74816-68-5
Molecular Formula:C₁₆H₁₃ClN₄O₂
Molecular Weight:328.758
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-Chloro-2,4-dioxo-1,3-dimethyl-6'-phenyl-1,2,3,4-tetrahydro-4',5-dipyrimidinyl

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Technology Process of 2'-Chloro-2,4-dioxo-1,3-dimethyl-6'-phenyl-1,2,3,4-tetrahydro-4',5-dipyrimidinyl

There total 3 articles about 2'-Chloro-2,4-dioxo-1,3-dimethyl-6'-phenyl-1,2,3,4-tetrahydro-4',5-dipyrimidinyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 74816-67-4
2,2',4-Trioxo-1,3-dimethyl-6'-phenyl-1,1',2,2',3,4-hexahydro-4',5-dipyrimidinyl

: 74816-68-5
2'-Chloro-2,4-dioxo-1,3-dimethyl-6'-phenyl-1,2,3,4-tetrahydro-4',5-dipyrimidinyl

Guidance literature:: With water; 2,3-Dimethylaniline; trichlorophosphate; for 4h; Heating;
DOI:10.1007/BF02401733

Reference yield:

: Benzalbisurea

: 74816-68-5
2'-Chloro-2,4-dioxo-1,3-dimethyl-6'-phenyl-1,2,3,4-tetrahydro-4',5-dipyrimidinyl

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / HCl / butan-1-ol / 7 h / Heating

2: 92 percent / POCl₃, H₂O, dimethylaniline / 4 h / Heating

With hydrogenchloride; water; 2,3-Dimethylaniline; trichlorophosphate; In butan-1-ol;
DOI:10.1007/BF02401733

Reference yield:

: 36980-95-7
5-(1,3-Dimethyl-2,4-dioxopyrimidil)methyl ketone

: 74816-68-5
2'-Chloro-2,4-dioxo-1,3-dimethyl-6'-phenyl-1,2,3,4-tetrahydro-4',5-dipyrimidinyl

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / HCl / butan-1-ol / 7 h / Heating

2: 92 percent / POCl₃, H₂O, dimethylaniline / 4 h / Heating

With hydrogenchloride; water; 2,3-Dimethylaniline; trichlorophosphate; In butan-1-ol;
DOI:10.1007/BF02401733