pentacarbonyl(sym-di-p-tolylthiourea)tungsten⁽⁰⁾

Base Information

Chemical Name:pentacarbonyl(sym-di-p-tolylthiourea)tungsten⁽⁰⁾
CAS No.:796047-41-1
Molecular Formula:C₂₀H₁₆N₂O₅SW
Molecular Weight:580.273
Hs Code.:

pentacarbonyl(sym-di-p-tolylthiourea)tungsten<sup>(0)</sup>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentacarbonyl(sym-di-p-tolylthiourea)tungsten⁽⁰⁾

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Technology Process of pentacarbonyl(sym-di-p-tolylthiourea)tungsten⁽⁰⁾

There total 1 articles about pentacarbonyl(sym-di-p-tolylthiourea)tungsten⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.2%

: 14040-11-0
tungsten hexacarbonyl

: 621-01-2
N,N'-Bis(p-tolyl)thiourea

: 796047-41-1
pentacarbonyl(sym-di-p-tolylthiourea)tungsten⁽⁰⁾

Guidance literature:: In toluene; under Ar or vac., 1 equiv. of S-compd., reflux for 4.5 h; soln. was cooled and evapd. in vac., solid was washed with petroleum ether (40-60 °C), recrystn. from benzene, elem. anal.;
DOI:10.1515/znb-2004-0512

Reference yield: 58.6%

: 796047-41-1
pentacarbonyl(sym-di-p-tolylthiourea)tungsten⁽⁰⁾

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 796047-66-0
tetracarbonyl(sym-p-tolylthiourea)diiodotungsten⁽⁰⁾

Guidance literature:: In benzene; under Ar or vac., 1 equiv. of halogen, excess of halogen led to an unidentified sticky product, room temp.; ppt. was sepd., washed repeatedly with hexane, solid was dissolved in min. amt. of benzene, re-pptd. with hexane, ppt. was dried in vac., elem. anal.;
DOI:10.1515/znb-2004-0512

Reference yield: 54.6%

: 796047-41-1
pentacarbonyl(sym-di-p-tolylthiourea)tungsten⁽⁰⁾

: 7726-95-6
bromine

: 796047-71-7
tetracarbonyl(sym-p-tolylthiourea)dibromotungsten⁽⁰⁾

Guidance literature:: In benzene; under Ar or vac., 1 equiv. of halogen, excess of halogen led to an unidentified sticky product, room temp.; ppt. was sepd., washed repeatedly with hexane, solid was dissolved in min. amt. of benzene, re-pptd. with hexane, ppt. was dried in vac., elem. anal.;
DOI:10.1515/znb-2004-0512