2,4-diphenyl-1,3,2,4-dithiadistibetane

Base Information

Chemical Name:2,4-diphenyl-1,3,2,4-dithiadistibetane
CAS No.:895166-03-7
Molecular Formula:C₁₂H₁₀S₂Sb₂
Molecular Weight:461.843
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-diphenyl-1,3,2,4-dithiadistibetane

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Technology Process of 2,4-diphenyl-1,3,2,4-dithiadistibetane

There total 2 articles about 2,4-diphenyl-1,3,2,4-dithiadistibetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: bis[(4-methylbenzoyl)thio]phenylantimony

: 895166-03-7
2,4-diphenyl-1,3,2,4-dithiadistibetane

Guidance literature:: With piperidine; In dichloromethane; byproducts: piperidinium 4-methylbenzenecarbothioate, N-(4-methylbenzoyl)piperidine; to a suspn. of Sb-compound in CH2Cl2 was added a soln. of piperidine in CH2Cl2 at room temp., the mixt. was stirred at 0°C for 6 h; filtered;
DOI:10.1002/hlca.200690070

Reference yield:

: 42967-76-0
piperidinium 4-methylbenzenecarbodithiolate

: 5035-52-9
dichlorophenylstibine

: 895166-03-7
2,4-diphenyl-1,3,2,4-dithiadistibetane

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: piperidine / diethyl ether

With piperidine; In diethyl ether; dichloromethane;
DOI:10.1002/hlca.200690070