2-benzoyl-2-methyladamantane

Base Information

Chemical Name:2-benzoyl-2-methyladamantane
CAS No.:219812-03-0
Molecular Formula:C₁₈H₂₂O
Molecular Weight:254.372
Hs Code.:

Synonyms:

Suppliers and Price of 2-benzoyl-2-methyladamantane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzoyl-2-methyladamantane

Chemical Property:

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Technology Process of 2-benzoyl-2-methyladamantane

There total 7 articles about 2-benzoyl-2-methyladamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68157-27-7
adamantan-2-yl(phenyl)methanone

: 74-88-4
methyl iodide

: 219812-03-0
2-benzoyl-2-methyladamantane

Guidance literature:: With sodium hydride; Yield given; Multistep reaction; 1.) 1,2-dimethoxyethane, reflux, 4 h, 2.) 1,2-dimethoxyethane, reflux, 1.5 h;
DOI:10.1021/ja9823013

Reference yield:

: 40079-92-3
2-adamantanecarbonyl chloride

: 219812-03-0
2-benzoyl-2-methyladamantane

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃ / 5 h / Ambient temperature

2: 1.) NaH / 1.) 1,2-dimethoxyethane, reflux, 4 h, 2.) 1,2-dimethoxyethane, reflux, 1.5 h

With aluminium trichloride; sodium hydride;
DOI:10.1021/ja9823013

Reference yield:

: 15897-81-1
adamantane-2-carboxylic acid

: 219812-03-0
2-benzoyl-2-methyladamantane

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 2 h / Heating

2: AlCl₃ / 5 h / Ambient temperature

3: 1.) NaH / 1.) 1,2-dimethoxyethane, reflux, 4 h, 2.) 1,2-dimethoxyethane, reflux, 1.5 h

With aluminium trichloride; thionyl chloride; sodium hydride;
DOI:10.1021/ja9823013