(Rax)-2-[N-(o-carboranylmethyl)-N-(4-fluorophenyl)amino]dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepane

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Chemical Name:(Rax)-2-[N-(o-carboranylmethyl)-N-(4-fluorophenyl)amino]dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepane
CAS No.:1272384-56-1
Molecular Formula:C₂₉H₂₉B₁₀FNO₂P
Molecular Weight:581.637
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Rax)-2-[N-(o-carboranylmethyl)-N-(4-fluorophenyl)amino]dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepane

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Technology Process of (Rax)-2-[N-(o-carboranylmethyl)-N-(4-fluorophenyl)amino]dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepane

There total 1 articles about (Rax)-2-[N-(o-carboranylmethyl)-N-(4-fluorophenyl)amino]dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 171878-71-0,137156-22-0,155613-52-8
(Ra)-2-chlorodinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepane

: 1272384-54-9
N-(o-carboranylmethyl)-N-(4-fluorophenyl)amine

: 1272384-56-1
(Rax)-2-[N-(o-carboranylmethyl)-N-(4-fluorophenyl)amino]dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepane

Guidance literature:: With (C₂H₅)3N; In benzene; byproducts: HN(C2H5)3Cl; (Ar); Et3N and carborane amine were added to soln. of BINOL in benzene, stirred for 10 min at 20°C, heated to reflux, cooled to room temp.; filtered off, column flash-chromy. (silica, benzene), elem. anal.;
DOI:10.1007/s11172-010-0321-y