N-(o-carboranylmethyl)-N-(4-fluorophenyl)amine

Base Information

Chemical Name:N-(o-carboranylmethyl)-N-(4-fluorophenyl)amine
CAS No.:1272384-54-9
Molecular Formula:C₉H₁₈B₁₀FN
Molecular Weight:267.357
Hs Code.:

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Chemical Property of N-(o-carboranylmethyl)-N-(4-fluorophenyl)amine

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Technology Process of N-(o-carboranylmethyl)-N-(4-fluorophenyl)amine

There total 1 articles about N-(o-carboranylmethyl)-N-(4-fluorophenyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 850071-63-5
1-(trifluoromethanesulfonylmethyl)-1,2-dicarba-closo-dodecaborane⁽¹²⁾

: 371-40-4
4-fluoroaniline

: 1272384-54-9
N-(o-carboranylmethyl)-N-(4-fluorophenyl)amine

Guidance literature:: With CH₃COONa; In acetonitrile; (Ar); mixt. of triflate, amine, NaOAc and MeCN was refluxed for 4-8 h; water was added, extd. with EtOAc, washed with water, dried over Na2SO4,filtered, evapd. in vac., column chromy. (silica, heptane/EtOAc, 10:1), elem. anal.;
DOI:10.1007/s11172-010-0321-y

Reference yield: 85.0%

: 171878-71-0,137156-22-0,155613-52-8
(Ra)-2-chlorodinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepane

: 1272384-54-9
N-(o-carboranylmethyl)-N-(4-fluorophenyl)amine

: 1272384-56-1
(Rax)-2-[N-(o-carboranylmethyl)-N-(4-fluorophenyl)amino]dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepane

Guidance literature:: With (C₂H₅)3N; In benzene; byproducts: HN(C2H5)3Cl; (Ar); Et3N and carborane amine were added to soln. of BINOL in benzene, stirred for 10 min at 20°C, heated to reflux, cooled to room temp.; filtered off, column flash-chromy. (silica, benzene), elem. anal.;
DOI:10.1007/s11172-010-0321-y