Technology Process of C24H36O2Si
There total 5 articles about C24H36O2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
hexane;
for 2h;
Inert atmosphere;
Reflux;
DOI:10.1021/ja201467z
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / hexane; tert-butyl methyl ether / 0.17 h / -78 °C / Inert atmosphere
1.2: 0.67 h / 0 - 20 °C / Inert atmosphere
2.1: sodium hydride / hexane / 2 h / Inert atmosphere; Reflux
With
n-butyllithium; sodium hydride;
In
hexane; tert-butyl methyl ether;
DOI:10.1021/ja201467z
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere
1.2: 12 h / 0 - 70 °C / Inert atmosphere
2.1: Oxone; Shi's ketone; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; potassium carbonate; acetic acid; potassium hydroxide / Dimethoxymethane; acetonitrile / 3 h / -10 °C / Inert atmosphere; aq. buffer
3.1: n-butyllithium / hexane; tert-butyl methyl ether / 0.17 h / -78 °C / Inert atmosphere
3.2: 0.67 h / 0 - 20 °C / Inert atmosphere
4.1: sodium hydride / hexane / 2 h / Inert atmosphere; Reflux
With
Oxone; n-butyllithium; Shi's ketone; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; sodium hydride; potassium carbonate; acetic acid; potassium hydroxide;
In
tetrahydrofuran; Dimethoxymethane; hexane; tert-butyl methyl ether; acetonitrile;
DOI:10.1021/ja201467z
