Benzoic acid 6-[(S)-((1R,4S,7R,8R,9S)-5-hydroxy-7-methoxy-10-methyl-2-oxo-6-oxa-3,10-diaza-tricyclo[6.2.1.0^4,9]undec-3-yl)-methoxycarbonyl-methyl]-2,4-dimethoxy-3-methyl-phenyl ester

Base Information

• Chemical Name: Benzoic acid 6-[(S)-((1R,4S,7R,8R,9S)-5-hydroxy-7-methoxy-10-methyl-2-oxo-6-oxa-3,10-diaza-tricyclo[6.2.1.0^4,9]undec-3-yl)-methoxycarbonyl-methyl]-2,4-dimethoxy-3-methyl-phenyl ester
• CAS No.: 97911-69-8
• Molecular Formula: C₂₉H₃₄N₂O₁₀
• Molecular Weight: 570.596

Synonyms:

Chemical Property of Benzoic acid 6-[(S)-((1R,4S,7R,8R,9S)-5-hydroxy-7-methoxy-10-methyl-2-oxo-6-oxa-3,10-diaza-tricyclo[6.2.1.0^4,9]undec-3-yl)-methoxycarbonyl-methyl]-2,4-dimethoxy-3-methyl-phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Benzoic acid 6-[(S)-((1R,4S,7R,8R,9S)-5-hydroxy-7-methoxy-10-methyl-2-oxo-6-oxa-3,10-diaza-tricyclo[6.2.1.0^4,9]undec-3-yl)-methoxycarbonyl-methyl]-2,4-dimethoxy-3-methyl-phenyl ester

There total 1 articles about Benzoic acid 6-[(S)-((1R,4S,7R,8R,9S)-5-hydroxy-7-methoxy-10-methyl-2-oxo-6-oxa-3,10-diaza-tricyclo[6.2.1.0^4,9]undec-3-yl)-methoxycarbonyl-methyl]-2,4-dimethoxy-3-methyl-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Benzoic acid 2,4-dimethoxy-6-[(S)-methoxycarbonyl-((1R,4R,7S,8S)-9-methyl-2-oxo-3,9-diaza-tricyclo[5.2.1.04,8]dec-5-en-3-yl)-methyl]-3-methyl-phenyl ester; hydrochloride (97911-68-7) → Benzoic acid 6-[(S)-((1R,4S,7R,8R,9S)-5-hydroxy-7-methoxy-10-methyl-2-oxo-6-oxa-3,10-diaza-tricyclo[6.2.1.04,9]undec-3-yl)-methoxycarbonyl-methyl]-2,4-dimethoxy-3-methyl-phenyl ester (97911-69-8,97949-83-2)

Guidance literature:

With oil scarlet; hydrogen; ozone; palladium on activated charcoal; Yield given. Multistep reaction; 1) MeOH, -78 deg C 2) -78 to 25 deg C;

DOI:10.1016/S0040-4039(00)98339-4

Reference yield:

Benzoic acid 6-[(S)-((1R,4S,7R,8R,9S)-5-hydroxy-7-methoxy-10-methyl-2-oxo-6-oxa-3,10-diaza-tricyclo[6.2.1.04,9]undec-3-yl)-methoxycarbonyl-methyl]-2,4-dimethoxy-3-methyl-phenyl ester (97911-69-8,97949-83-2) → Benzoic acid 6-[(S)-((1R,4S,5R,7R,8R,9S)-5-chloro-7-methoxy-10-methyl-2-oxo-6-oxa-3,10-diaza-tricyclo[6.2.1.04,9]undec-3-yl)-methoxycarbonyl-methyl]-2,4-dimethoxy-3-methyl-phenyl ester (97911-71-2)

Guidance literature:

With tetrachloromethane; Hexamethylphosphorous triamide; In dichloromethane; at -78 - 25 ℃;

DOI:10.1016/S0040-4039(00)98339-4

Reference yield:

Benzoic acid 6-[(S)-((1R,4S,7R,8R,9S)-5-hydroxy-7-methoxy-10-methyl-2-oxo-6-oxa-3,10-diaza-tricyclo[6.2.1.04,9]undec-3-yl)-methoxycarbonyl-methyl]-2,4-dimethoxy-3-methyl-phenyl ester (97911-69-8,97949-83-2) → C29H32N2O9 (97911-72-3)

Guidance literature:

Multi-step reaction with 2 steps

1: (Me₂N)3P, CCl₄ / CH₂Cl₂ / -78 - 25 °C

2: SnCl₄ / -78 - 0 °C

With tetrachloromethane; tin(IV) chloride; Hexamethylphosphorous triamide; In dichloromethane;

DOI:10.1016/S0040-4039(00)98339-4

upstream raw materials:

Benzoic acid 2,4-dimethoxy-6-[(S)-methoxycarbonyl-((1R,4R,7S,8S)-9-methyl-2-oxo-3,9-diaza-tricyclo[5.2.1.0^4,8]dec-5-en-3-yl)-methyl]-3-methyl-phenyl ester; hydrochloride

Downstream raw materials:

C₂₈H₃₀N₂O₉

Benzoic acid 6-[(S)-((1R,4S,5R,7R,8R,9S)-5-chloro-7-methoxy-10-methyl-2-oxo-6-oxa-3,10-diaza-tricyclo[6.2.1.0^4,9]undec-3-yl)-methoxycarbonyl-methyl]-2,4-dimethoxy-3-methyl-phenyl ester

C₂₉H₃₂N₂O₉

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