benzyl O-β-D-glucopyranosyl-(1->4)-O-β-D-glucopyranosyl-(1->4)-O-(2,3,6-O-tri-O-benzyl-β-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:benzyl O-β-D-glucopyranosyl-(1->4)-O-β-D-glucopyranosyl-(1->4)-O-(2,3,6-O-tri-O-benzyl-β-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:88567-42-4
Molecular Formula:C₇₃H₈₄O₂₁
Molecular Weight:1297.46
Hs Code.:

benzyl O-β-D-glucopyranosyl-(1->4)-O-β-D-glucopyranosyl-(1->4)-O-(2,3,6-O-tri-O-benzyl-β-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Suppliers and Price of benzyl O-β-D-glucopyranosyl-(1->4)-O-β-D-glucopyranosyl-(1->4)-O-(2,3,6-O-tri-O-benzyl-β-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of benzyl O-β-D-glucopyranosyl-(1->4)-O-β-D-glucopyranosyl-(1->4)-O-(2,3,6-O-tri-O-benzyl-β-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of benzyl O-β-D-glucopyranosyl-(1->4)-O-β-D-glucopyranosyl-(1->4)-O-(2,3,6-O-tri-O-benzyl-β-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 2 articles about benzyl O-β-D-glucopyranosyl-(1->4)-O-β-D-glucopyranosyl-(1->4)-O-(2,3,6-O-tri-O-benzyl-β-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62867-73-6
benzyl 2,3,6-tri-O-benzyl-4-O-(2′,3′-di-O-benzyl-4′,6′-Obenzylidene-β-D-glucopyranosyl)-β-D-glucopyranoside

: 88567-42-4
benzyl O-β-D-glucopyranosyl-(1->4)-O-β-D-glucopyranosyl-(1->4)-O-(2,3,6-O-tri-O-benzyl-β-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / sodium cyanoborohydride, molecular sieves 3A, hydrochloric acid/Et₂O / CH₂Cl₂; various solvent(s); tetrahydrofuran / 1 h / 0 °C

2: 1.) mercuric cyanide; 2.) potassium iodide, sodium methoxide / 1.) benzene, nitromethane, 65 deg C, 66 h; 2.) chloroform, water, methanol, 2 h, r.t.

With hydrogenchloride; diethyl ether; 3 A molecular sieve; sodium methylate; mercury(II) cyanide; sodium cyanoborohydride; potassium iodide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0008-6215(83)84014-2

Reference yield:

: 88559-76-6
benzyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranoside

: 14227-66-8
acetobromocellobiose

: 88567-42-4
benzyl O-β-D-glucopyranosyl-(1->4)-O-β-D-glucopyranosyl-(1->4)-O-(2,3,6-O-tri-O-benzyl-β-D-glucopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With sodium methylate; mercury(II) cyanide; potassium iodide; Yield given. Multistep reaction; 1.) benzene, nitromethane, 65 deg C, 66 h; 2.) chloroform, water, methanol, 2 h, r.t.;
DOI:10.1016/0008-6215(83)84014-2