C₃₅H₄₃NO₃

Base Information

• Chemical Name: C₃₅H₄₃NO₃
• CAS No.: 211100-71-9
• Molecular Formula: C₃₅H₄₃NO₃
• Molecular Weight: 525.731
• Mol file: 211100-71-9.mol

Synonyms:

Chemical Property of C₃₅H₄₃NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₄₃NO₃

There total 10 articles about C₃₅H₄₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexanedione monoethylene ketal (4746-97-8) → C35H43NO3 (211100-71-9)

Guidance literature:

Multi-step reaction with 10 steps

1: 60 percent / tert-BuOK, KI / 2-methyl-propan-2-ol / Ambient temperature

2: NH₃ / methanol / 100 °C / 15514.4 Torr

3: Ag₂CO₃ / CHCl₃ / Heating

4: HCl / methanol / Heating

5: NaH / tetrahydrofuran / Heating

6: TsOH / benzene / Heating

7: (Me₂N)C=NH / CH₂Cl₂ / 48 h / -20 °C

8: Et₃N, DMAP / CH₂Cl₂ / Ambient temperature

9: NaOAc, AcOH / Heating

10: tert-BuOK / tetrahydrofuran / Ambient temperature

With hydrogenchloride; dmap; potassium tert-butylate; ammonia; sodium acetate; sodium hydride; toluene-4-sulfonic acid; acetic acid; triethylamine; silver carbonate; potassium iodide; N,N,N',N'-tetramethylguanidine; In tetrahydrofuran; methanol; dichloromethane; chloroform; tert-butyl alcohol; benzene;

DOI:10.1039/a801748d

Reference yield:

6,9-dioxadispiro[2.1.45.33]dodecan-12-one (211100-59-3) → C35H43NO3 (211100-71-9)

Guidance literature:

Multi-step reaction with 9 steps

1: NH₃ / methanol / 100 °C / 15514.4 Torr

2: Ag₂CO₃ / CHCl₃ / Heating

3: HCl / methanol / Heating

4: NaH / tetrahydrofuran / Heating

5: TsOH / benzene / Heating

6: (Me₂N)C=NH / CH₂Cl₂ / 48 h / -20 °C

7: Et₃N, DMAP / CH₂Cl₂ / Ambient temperature

8: NaOAc, AcOH / Heating

9: tert-BuOK / tetrahydrofuran / Ambient temperature

With hydrogenchloride; dmap; potassium tert-butylate; ammonia; sodium acetate; sodium hydride; toluene-4-sulfonic acid; acetic acid; triethylamine; silver carbonate; N,N,N',N'-tetramethylguanidine; In tetrahydrofuran; methanol; dichloromethane; chloroform; benzene;

DOI:10.1039/a801748d

Reference yield:

C12H13NO2 → C35H43NO3 (211100-71-9)

Guidance literature:

Multi-step reaction with 6 steps

1: NaH / tetrahydrofuran / Heating

2: TsOH / benzene / Heating

3: (Me₂N)C=NH / CH₂Cl₂ / 48 h / -20 °C

4: Et₃N, DMAP / CH₂Cl₂ / Ambient temperature

5: NaOAc, AcOH / Heating

6: tert-BuOK / tetrahydrofuran / Ambient temperature

With dmap; potassium tert-butylate; sodium acetate; sodium hydride; toluene-4-sulfonic acid; acetic acid; triethylamine; N,N,N',N'-tetramethylguanidine; In tetrahydrofuran; dichloromethane; benzene;

DOI:10.1039/a801748d

upstream raw materials:

ethyltriphenylphosphonium bromide

C₃₃H₃₉NO₄

cyclohexanedione monoethylene ketal

6,9-dioxadispiro[2.1.4⁵.3³]dodecan-12-one