Technology Process of C32H57N2O8P
There total 6 articles about C32H57N2O8P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 10.36 g / pyridine / 4 h / 60 °C
2: 14.42 g / pyridine / benzene / 1 h / Ambient temperature
3: 4.3 g / boric acid, (OCH3)3B / 3 h / Heating
4: 1.) pyridine, 2.) O.1M aq. KCl / 1.) room temp., 1 h, 2.) room temp., 1 h
5: 2.) Ag2CO3 / 1.) butan-2-one, 2.) 80 deg C, 1 h, CHCl3
With
pyridine; Trimethyl borate; potassium chloride; boric acid; silver carbonate;
In
benzene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 7 g / NaHCO3 / methanol; H2O; toluene / 24 h / Ambient temperature
2: 10.36 g / pyridine / 4 h / 60 °C
3: 14.42 g / pyridine / benzene / 1 h / Ambient temperature
4: 4.3 g / boric acid, (OCH3)3B / 3 h / Heating
5: 1.) pyridine, 2.) O.1M aq. KCl / 1.) room temp., 1 h, 2.) room temp., 1 h
6: 2.) Ag2CO3 / 1.) butan-2-one, 2.) 80 deg C, 1 h, CHCl3
With
pyridine; Trimethyl borate; potassium chloride; boric acid; sodium hydrogencarbonate; silver carbonate;
In
methanol; water; toluene; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 14.42 g / pyridine / benzene / 1 h / Ambient temperature
2: 4.3 g / boric acid, (OCH3)3B / 3 h / Heating
3: 1.) pyridine, 2.) O.1M aq. KCl / 1.) room temp., 1 h, 2.) room temp., 1 h
4: 2.) Ag2CO3 / 1.) butan-2-one, 2.) 80 deg C, 1 h, CHCl3
With
pyridine; Trimethyl borate; potassium chloride; boric acid; silver carbonate;
In
benzene;